Technology Process of C31H28N6O9
There total 9 articles about C31H28N6O9 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
1,4-dioxane;
at 20 ℃;
for 17h;
DOI:10.1021/ol026815p
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 70 percent / sodium dithionite / ethanol; H2O / 0.5 h / 20 °C
2.1: Ph3P; CCl4 / CH2Cl2 / 3 h / Heating
2.2: 12 percent / DBU / CH2Cl2 / 13 h / 20 °C
3.1: 76 percent / KF / ethanol / 20 h / Heating
4.1: 39 percent / DEAD; Ph2PC6H4-polymer / CH2Cl2 / 4 h / 20 °C
5.1: 98 percent / HCl / dioxane / 17 h / 20 °C
With
hydrogenchloride; tetrachloromethane; potassium fluoride; sodium dithionite; Ph2PC6H4-polymer; triphenylphosphine; diethylazodicarboxylate;
In
1,4-dioxane; ethanol; dichloromethane; water;
4.1: Mitsunobu alkylation;
DOI:10.1021/ol026815p
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: Ph3P; CCl4 / CH2Cl2 / 3 h / Heating
1.2: 12 percent / DBU / CH2Cl2 / 13 h / 20 °C
2.1: 76 percent / KF / ethanol / 20 h / Heating
3.1: 39 percent / DEAD; Ph2PC6H4-polymer / CH2Cl2 / 4 h / 20 °C
4.1: 98 percent / HCl / dioxane / 17 h / 20 °C
With
hydrogenchloride; tetrachloromethane; potassium fluoride; Ph2PC6H4-polymer; triphenylphosphine; diethylazodicarboxylate;
In
1,4-dioxane; ethanol; dichloromethane;
3.1: Mitsunobu alkylation;
DOI:10.1021/ol026815p