2-dimethoxymethyl-3-hydroxybenzenecarbaldehyde

Base Information

Chemical Name:2-dimethoxymethyl-3-hydroxybenzenecarbaldehyde
CAS No.:386708-36-7
Molecular Formula:C₁₀H₁₂O₄
Molecular Weight:196.203
Hs Code.:

Synonyms:2-dimethoxymethyl-3-hydroxybenzenecarbaldehyde

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Chemical Property of 2-dimethoxymethyl-3-hydroxybenzenecarbaldehyde

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Technology Process of 2-dimethoxymethyl-3-hydroxybenzenecarbaldehyde

There total 4 articles about 2-dimethoxymethyl-3-hydroxybenzenecarbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 386708-35-6
2-dimethoxymethyl-3-hydroxymethylphenol

: 386708-36-7
2-dimethoxymethyl-3-hydroxybenzenecarbaldehyde

Guidance literature:: With manganese(IV) oxide; In acetone; at 20 ℃;
DOI:10.1271/bbb.65.2315

Reference yield:

: 19438-10-9
methyl 3-hydroxybenzoate

: 386708-36-7
2-dimethoxymethyl-3-hydroxybenzenecarbaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: 29 percent / aq. polyphosphoric acid / 110 °C

2: montmorillonite K₁₀ / hexane; CH₂Cl₂

3: LiAlH₄ / diethyl ether / 0 °C

4: 82 percent / MnO₂ / acetone / 20 °C

With manganese(IV) oxide; lithium aluminium tetrahydride; PPA; Montmorillonite K₁₀; In diethyl ether; hexane; dichloromethane; acetone;
DOI:10.1271/bbb.65.2315

Reference yield:

: 131524-43-1
methyl 2-formyl-3-hydroxybenzoate

: 386708-36-7
2-dimethoxymethyl-3-hydroxybenzenecarbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: montmorillonite K₁₀ / hexane; CH₂Cl₂

2: LiAlH₄ / diethyl ether / 0 °C

3: 82 percent / MnO₂ / acetone / 20 °C

With manganese(IV) oxide; lithium aluminium tetrahydride; Montmorillonite K₁₀; In diethyl ether; hexane; dichloromethane; acetone;
DOI:10.1271/bbb.65.2315