4-(4-methoxyphenyl)-6,6-dimethyl-3-methylene-2-(trimethylsiloxy)-1,2-oxazinane

Base Information

Chemical Name:4-(4-methoxyphenyl)-6,6-dimethyl-3-methylene-2-(trimethylsiloxy)-1,2-oxazinane
CAS No.:1198015-22-3
Molecular Formula:C₁₇H₂₇NO₃Si
Molecular Weight:321.492
Hs Code.:

Synonyms:4-(4-methoxyphenyl)-6,6-dimethyl-3-methylene-2-(trimethylsiloxy)-1,2-oxazinane

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Chemical Property of 4-(4-methoxyphenyl)-6,6-dimethyl-3-methylene-2-(trimethylsiloxy)-1,2-oxazinane

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Technology Process of 4-(4-methoxyphenyl)-6,6-dimethyl-3-methylene-2-(trimethylsiloxy)-1,2-oxazinane

There total 1 articles about 4-(4-methoxyphenyl)-6,6-dimethyl-3-methylene-2-(trimethylsiloxy)-1,2-oxazinane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 929878-88-6
4-(4-methoxyphenyl)-3,6,6-trimethyl-5,6-dihydro-4H-1,2-oxazine 2-oxide

: 2857-97-8
trimethylsilyl bromide

: 1198015-22-3
4-(4-methoxyphenyl)-6,6-dimethyl-3-methylene-2-(trimethylsiloxy)-1,2-oxazinane

Guidance literature:: With triethylamine; In dichloromethane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1055/s-0029-1216907

Reference yield: 72.0%

: 1198015-22-3
4-(4-methoxyphenyl)-6,6-dimethyl-3-methylene-2-(trimethylsiloxy)-1,2-oxazinane

: (4-(4-methoxyphenyl)-6,6-dimethyl-5,6-dihydro-4H-1,2-oxazin-3-yl)methyl nitrate

Guidance literature:: With chromium(III) nitrate nonahydrate; In tetrahydrofuran; dichloromethane; at 20 ℃; for 2h;
DOI:10.1039/c6ob00388e

Reference yield: 63.0%

: 1198015-22-3
4-(4-methoxyphenyl)-6,6-dimethyl-3-methylene-2-(trimethylsiloxy)-1,2-oxazinane

: 407-25-0
trifluoroacetic anhydride

: 1198015-27-8
[4-(4-methoxyphenyl)-6,6-dimethyl-5,6-dihydro-4H-1,2-oxazin-3-yl]methanol

Guidance literature:: 4-(4-methoxyphenyl)-6,6-dimethyl-3-methylene-2-(trimethylsiloxy)-1,2-oxazinane; trifluoroacetic anhydride; In dichloromethane; at -78 - 20 ℃; Inert atmosphere;

With methanol; potassium carbonate; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1055/s-0029-1216907