α-(pentamethylphenyl)pentachlorophenylacetic acid

Base Information

Chemical Name:α-(pentamethylphenyl)pentachlorophenylacetic acid
CAS No.:150884-37-0
Molecular Formula:C₁₉H₁₇Cl₅O₂
Molecular Weight:454.608
Hs Code.:

Synonyms:α-(pentamethylphenyl)pentachlorophenylacetic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of α-(pentamethylphenyl)pentachlorophenylacetic acid

Chemical Property:

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Technology Process of α-(pentamethylphenyl)pentachlorophenylacetic acid

There total 3 articles about α-(pentamethylphenyl)pentachlorophenylacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 150884-36-9
isopropyl α-(pentamethylphenyl)pentachlorophenylacetate

: 150884-37-0
α-(pentamethylphenyl)pentachlorophenylacetic acid

Guidance literature:: With sulfuric acid; trifluoroacetic acid; for 1h; Ambient temperature;
DOI:10.1055/s-1993-25911

Reference yield:

: 118-74-1,67471-27-6
hexachlorobenzene

: 150884-37-0
α-(pentamethylphenyl)pentachlorophenylacetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 1) Mg / 1) THF, benzene, 2) 0 deg C, 1 h

2: 1) Mg, 1,2-dibromoethane / 1) THF, 2) benzene, r.t., 4 h

3: 64 percent / CF₃COOH, H₂SO₄ / 1 h / Ambient temperature

With sulfuric acid; magnesium; ethylene dibromide; trifluoroacetic acid;
DOI:10.1055/s-1993-25911

Reference yield:

: 150884-35-8
ISOPROPYL α-oxopentachlorophenylacetate

: 150884-37-0
α-(pentamethylphenyl)pentachlorophenylacetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1) Mg, 1,2-dibromoethane / 1) THF, 2) benzene, r.t., 4 h

2: 64 percent / CF₃COOH, H₂SO₄ / 1 h / Ambient temperature

With sulfuric acid; magnesium; ethylene dibromide; trifluoroacetic acid;
DOI:10.1055/s-1993-25911