<1R-(1α,2α,3α)>-2-(hydroxymethyl)-1--N-(p-methoxybenzyl)hydroxycarboxamido>-3-(2-propyl)cyclopropane

Base Information

Chemical Name:<1R-(1α,2α,3α)>-2-(hydroxymethyl)-1--N-(p-methoxybenzyl)hydroxycarboxamido>-3-(2-propyl)cyclopropane
CAS No.:149859-31-4
Molecular Formula:C₂₄H₃₁NO₅
Molecular Weight:413.514
Hs Code.:

<1R-(1α,2α,3α)>-2-(hydroxymethyl)-1-<N-<O-(p-methoxybenzyl)>-N-(p-methoxybenzyl)hydroxycarboxamido>-3-(2-propyl)cyclopropane

Synonyms:<1R-(1α,2α,3α)>-2-(hydroxymethyl)-1--N-(p-methoxybenzyl)hydroxycarboxamido>-3-(2-propyl)cyclopropane

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Chemical Property of <1R-(1α,2α,3α)>-2-(hydroxymethyl)-1--N-(p-methoxybenzyl)hydroxycarboxamido>-3-(2-propyl)cyclopropane

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Technology Process of <1R-(1α,2α,3α)>-2-(hydroxymethyl)-1--N-(p-methoxybenzyl)hydroxycarboxamido>-3-(2-propyl)cyclopropane

There total 6 articles about <1R-(1α,2α,3α)>-2-(hydroxymethyl)-1--N-(p-methoxybenzyl)hydroxycarboxamido>-3-(2-propyl)cyclopropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82290-65-1
(Z)-4-methylpent-2-en-1-ol

: 149859-31-4
<1R-(1α,2α,3α)>-2-(hydroxymethyl)-1--N-(p-methoxybenzyl)hydroxycarboxamido>-3-(2-propyl)cyclopropane

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / N,N-dimethylaniline, Et₃N / CH₂Cl₂ / 1) 0 deg C, 15 min, 2) r.t., 30 min

2: 85 percent / Rh₂<-CH₂-CH₂-CH(CO₂Me)-N=CO->4 / CH₂Cl₂ / Heating

3: 1) Me₃Al / 1) hexane, ClCH₂CH₂Cl, r.t., 1 h, 2) ClCH₂CH₂Cl, 83 deg C, 4 h

With trimethylaluminum; N,N-dimethyl-aniline; triethylamine; Rh2<-CH2-CH2-CH(CO2Me)-N=CO->4; In dichloromethane;
DOI:10.1016/S0040-4020(01)90212-1

Reference yield:

: 149859-29-0
4-methyl-2(Z)-pentenyl diazoacetate

: 149859-31-4
<1R-(1α,2α,3α)>-2-(hydroxymethyl)-1--N-(p-methoxybenzyl)hydroxycarboxamido>-3-(2-propyl)cyclopropane

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / Rh₂<-CH₂-CH₂-CH(CO₂Me)-N=CO->4 / CH₂Cl₂ / Heating

2: 1) Me₃Al / 1) hexane, ClCH₂CH₂Cl, r.t., 1 h, 2) ClCH₂CH₂Cl, 83 deg C, 4 h

With trimethylaluminum; Rh2<-CH2-CH2-CH(CO2Me)-N=CO->4; In dichloromethane;
DOI:10.1016/S0040-4020(01)90212-1

Reference yield:

: 21038-22-2
O-(4-methoxybenzyl)hydroxylamine

: 149859-31-4
<1R-(1α,2α,3α)>-2-(hydroxymethyl)-1--N-(p-methoxybenzyl)hydroxycarboxamido>-3-(2-propyl)cyclopropane

Guidance literature:: Multi-step reaction with 3 steps

1: 3 Angstroem molecular sieves / methanol / 25 °C

2: NaBH₃CN, HCl / methanol / 25 °C / pH 3

3: 1) Me₃Al / 1) hexane, ClCH₂CH₂Cl, r.t., 1 h, 2) ClCH₂CH₂Cl, 83 deg C, 4 h

With hydrogenchloride; 3 A molecular sieve; trimethylaluminum; sodium cyanoborohydride; In methanol;
DOI:10.1016/S0040-4020(01)90212-1