3,5-dimethoxybenzylmagnesium bromide

Base Information

• Chemical Name: 3,5-dimethoxybenzylmagnesium bromide
• CAS No.: 23815-45-4
• Molecular Formula: C₉H₁₁BrMgO₂
• Molecular Weight: 255.394

Synonyms:3,5-dimethoxybenzylmagnesium bromide

Chemical Property of 3,5-dimethoxybenzylmagnesium bromide

Chemical Property:

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Technology Process of 3,5-dimethoxybenzylmagnesium bromide

There total 1 articles about 3,5-dimethoxybenzylmagnesium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,5-dimethoxybenzyl bromide (877-88-3) → 3,5-dimethoxybenzylmagnesium bromide (23815-45-4)

Guidance literature:

With magnesium; In diethyl ether; toluene; at -10 ℃; for 3h; Inert atmosphere;

DOI:10.1039/d0ra02987d

Reference yield: 83.0%

3,5-dimethoxybenzylmagnesium bromide (23815-45-4) + 7-bromo-2,3-dihydro-1H-inden-1-one (125114-77-4) → 7-bromo-1-(3,5-dimethoxybenzyl)-2,3-dihydro-1H-inden-1-ol

Guidance literature:

In tetrahydrofuran; 2-methyltetrahydrofuran; at 0 - 20 ℃; for 2.5h;

Reference yield: 80.0%

geraniol acetate (74408-52-9,75157-67-4,74408-53-0) + 3,5-dimethoxybenzylmagnesium bromide (23815-45-4) → (E)-1-(4,8-dimethylnona-3,7-dien-1-yl)-3,5-dimethoxybenzene (1388152-64-4)

Guidance literature:

With dilithium tetrachlorocuprate; In tetrahydrofuran; at 0 ℃; for 2.33333h; Inert atmosphere;

DOI:10.1021/ja305851h

upstream raw materials:

3,5-dimethoxybenzyl bromide

Downstream raw materials:

2-(3,5-dimethoxy-benzyl)-5-isobutoxy-3-oxo-3,6-dihydro-2H-pyridine-1-carboxylic acid methyl ester

1,1-dimethyl-(3',5'-dimethoxyphenyl)ethanol

C₁₉H₂₈O₃

C₂₄H₃₆O₃

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