N-[(R,R)-2-(prop-2-ynyloxyethylamino)-1,2-diphenylethyl]-4-methyl benzenesulfonamide

Base Information

Chemical Name:N-[(R,R)-2-(prop-2-ynyloxyethylamino)-1,2-diphenylethyl]-4-methyl benzenesulfonamide
CAS No.:1448552-42-8
Molecular Formula:C₂₆H₂₈N₂O₃S
Molecular Weight:448.586
Hs Code.:

Synonyms:N-[(R,R)-2-(prop-2-ynyloxyethylamino)-1,2-diphenylethyl]-4-methyl benzenesulfonamide

Suppliers and Price of N-[(R,R)-2-(prop-2-ynyloxyethylamino)-1,2-diphenylethyl]-4-methyl benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[(R,R)-2-(prop-2-ynyloxyethylamino)-1,2-diphenylethyl]-4-methyl benzenesulfonamide

Chemical Property:

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Technology Process of N-[(R,R)-2-(prop-2-ynyloxyethylamino)-1,2-diphenylethyl]-4-methyl benzenesulfonamide

There total 2 articles about N-[(R,R)-2-(prop-2-ynyloxyethylamino)-1,2-diphenylethyl]-4-methyl benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-(prop-2-yn-1-yloxy)ethyl trifluoromethanesulfonate

: 144222-34-4
(R,R)-N-(p-toluenesulfonyl)-1,2-diphenylethylenediamine

: 1448552-42-8
N-[(R,R)-2-(prop-2-ynyloxyethylamino)-1,2-diphenylethyl]-4-methyl benzenesulfonamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 5 ℃; Inert atmosphere;
DOI:10.1016/j.tetasy.2013.05.022

Reference yield:

: 3973-18-0
2-(prop-2-ynyloxy)ethanol

: 1448552-42-8
N-[(R,R)-2-(prop-2-ynyloxyethylamino)-1,2-diphenylethyl]-4-methyl benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 2,6-dimethylpyridine / dichloromethane / 2.25 h / 0 - 22 °C / Inert atmosphere

2: triethylamine / dichloromethane / 0 - 5 °C / Inert atmosphere

With 2,6-dimethylpyridine; triethylamine; In dichloromethane;
DOI:10.1016/j.tetasy.2013.05.022

Reference yield: 60.5%

: 1448552-42-8
N-[(R,R)-2-(prop-2-ynyloxyethylamino)-1,2-diphenylethyl]-4-methyl benzenesulfonamide

: 66021-75-8
((2-azidoethoxy)methyl)benzene

: 1448552-44-0
C₃₅H₃₉N₅O₄S

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; tert-butyl alcohol; at 30 ℃; for 5h; Inert atmosphere;
DOI:10.1016/j.tetasy.2013.05.022