Ethyl 3-((aminocarbonyl)hydrazono)propionate

Base Information

Chemical Name:Ethyl 3-((aminocarbonyl)hydrazono)propionate
CAS No.:54977-77-4
Molecular Formula:C6H11 N3 O3
Molecular Weight:173.172
Hs Code.:2928000090
European Community (EC) Number:259-418-9
Mol file:54977-77-4.mol

Synonyms:Ethyl 3-((aminocarbonyl)hydrazono)propionate;54977-77-4;EINECS 259-418-9;ETHYL 3-[(AMINOCARBONYL)HYDRAZONO]PROPIONATE;AKOS000279228

Suppliers and Price of Ethyl 3-((aminocarbonyl)hydrazono)propionate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of Ethyl 3-((aminocarbonyl)hydrazono)propionate

Chemical Property:

PSA：93.78000
Density:1.278g/cm³
LogP:0.68490
XLogP3:-0.7
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:173.08004122
Heavy Atom Count:12
Complexity:191

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)CC=NNC(=O)N
Isomeric SMILES:CCOC(=O)C/C=N/NC(=O)N

Technology Process of Ethyl 3-((aminocarbonyl)hydrazono)propionate

There total 3 articles about Ethyl 3-((aminocarbonyl)hydrazono)propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 34780-29-5
3-oxo-propionic acid ethyl ester

: 4426-72-6,51433-48-8,57-56-7
hydrazine carboxamide

: 54977-77-4
3-semicarbazono-propionic acid ethyl ester

Guidance literature:: With sodium acetate; In ethanol; water;
DOI:10.1016/j.bmcl.2006.12.054

Reference yield:

: 10601-80-6
ethyl 3,3-diethoxypropanoate

: 54977-77-4
3-semicarbazono-propionic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: TFA / CH₂Cl₂; H₂O / 20 °C

2: 58 percent / NaOAc / ethanol; H₂O

With sodium acetate; trifluoroacetic acid; In ethanol; dichloromethane; water;
DOI:10.1016/j.bmcl.2006.12.054