ethyl 4-(benzyloxocarbonylamino)-2-methylene-5-(pyrrolidin-1-yl)-5-thioxopentanoate

Base Information

Chemical Name:ethyl 4-(benzyloxocarbonylamino)-2-methylene-5-(pyrrolidin-1-yl)-5-thioxopentanoate
CAS No.:1236108-95-4
Molecular Formula:C₂₀H₂₆N₂O₄S
Molecular Weight:390.503
Hs Code.:

Synonyms:ethyl 4-(benzyloxocarbonylamino)-2-methylene-5-(pyrrolidin-1-yl)-5-thioxopentanoate

Suppliers and Price of ethyl 4-(benzyloxocarbonylamino)-2-methylene-5-(pyrrolidin-1-yl)-5-thioxopentanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of ethyl 4-(benzyloxocarbonylamino)-2-methylene-5-(pyrrolidin-1-yl)-5-thioxopentanoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ethyl 4-(benzyloxocarbonylamino)-2-methylene-5-(pyrrolidin-1-yl)-5-thioxopentanoate

There total 1 articles about ethyl 4-(benzyloxocarbonylamino)-2-methylene-5-(pyrrolidin-1-yl)-5-thioxopentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1236108-91-0
benzyl (2-pyrrolidin-1-yl)-2-thioxoethylcarbamate

: 17435-72-2
ethyl 2-bromomethyl-2-propenoate

: 1236108-95-4
ethyl 4-(benzyloxocarbonylamino)-2-methylene-5-(pyrrolidin-1-yl)-5-thioxopentanoate

Guidance literature:: benzyl (2-pyrrolidin-1-yl)-2-thioxoethylcarbamate; ethyl 2-bromomethyl-2-propenoate; With ferric(III) bromide; In acetonitrile; at 45 - 50 ℃; Inert atmosphere;

With triethylamine; In tetrahydrofuran; toluene; at -78 - 45 ℃; Inert atmosphere;
DOI:10.1016/j.tetlet.2010.04.102