C₂₃H₂₈N₄O₅S

Base Information

Chemical Name:C₂₃H₂₈N₄O₅S
CAS No.:1443745-71-8
Molecular Formula:C₂₃H₂₈N₄O₅S
Molecular Weight:472.565
Hs Code.:

C<sub>23</sub>H<sub>28</sub>N<sub>4</sub>O<sub>5</sub>S

Synonyms:C₂₃H₂₈N₄O₅S

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Chemical Property of C₂₃H₂₈N₄O₅S

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Technology Process of C₂₃H₂₈N₄O₅S

There total 7 articles about C₂₃H₂₈N₄O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1443745-70-7
C₂₀H₂₁N₃O₆S

: 75-31-0
isopropylamine

: 1443745-71-8
C₂₃H₂₈N₄O₅S

Guidance literature:: With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dimethyl sulfoxide; at 20 ℃; for 16h;

Reference yield:

: 104-94-9
4-methoxy-aniline

: 1443745-71-8
C₂₃H₂₈N₄O₅S

Guidance literature:: Multi-step reaction with 7 steps

1.1: hydrogenchloride; sodium nitrite / ethanol; water / 0.33 h / 0 °C

1.2: 2 h / 0 °C

2.1: ammonium acetate; acetic acid / 0.75 h / 120 °C / Microwave irradiation

3.1: sulfur; morpholine / ethanol / 0.42 h / 130 °C / Microwave irradiation

4.1: dmap; di-tert-butyl dicarbonate / 4 h / 20 °C

5.1: caesium carbonate / N,N-dimethyl-formamide / 4 h / 0 - 20 °C

6.1: water; lithium hydroxide / tetrahydrofuran / 16 h / 20 °C

6.2: pH 6

7.1: N-ethyl-N,N-diisopropylamine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate / dimethyl sulfoxide / 16 h / 20 °C

With morpholine; hydrogenchloride; dmap; di-tert-butyl dicarbonate; ammonium acetate; water; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; caesium carbonate; sulfur; acetic acid; N-ethyl-N,N-diisopropylamine; lithium hydroxide; sodium nitrite; In tetrahydrofuran; ethanol; water; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 18794-95-1,77083-79-5,77098-98-7
3-oxo-2-(2-(4-methoxyphenyl)hydrazono)butanoic acid ethyl ester

: 1443745-71-8
C₂₃H₂₈N₄O₅S

Guidance literature:: Multi-step reaction with 6 steps

1.1: ammonium acetate; acetic acid / 0.75 h / 120 °C / Microwave irradiation

2.1: sulfur; morpholine / ethanol / 0.42 h / 130 °C / Microwave irradiation

3.1: dmap; di-tert-butyl dicarbonate / 4 h / 20 °C

4.1: caesium carbonate / N,N-dimethyl-formamide / 4 h / 0 - 20 °C

5.1: water; lithium hydroxide / tetrahydrofuran / 16 h / 20 °C

5.2: pH 6

6.1: N-ethyl-N,N-diisopropylamine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate / dimethyl sulfoxide / 16 h / 20 °C

With morpholine; dmap; di-tert-butyl dicarbonate; ammonium acetate; water; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; caesium carbonate; sulfur; acetic acid; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; ethanol; dimethyl sulfoxide; N,N-dimethyl-formamide;