C₂₇H₂₄F₄O₇S₂

Base Information

Chemical Name:C₂₇H₂₄F₄O₇S₂
CAS No.:1100362-45-5
Molecular Formula:C₂₇H₂₄F₄O₇S₂
Molecular Weight:600.609
Hs Code.:

C<sub>27</sub>H<sub>24</sub>F<sub>4</sub>O<sub>7</sub>S<sub>2</sub>

Synonyms:C₂₇H₂₄F₄O₇S₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₂₄F₄O₇S₂

Chemical Property:

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Technology Process of C₂₇H₂₄F₄O₇S₂

There total 8 articles about C₂₇H₂₄F₄O₇S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1100362-44-4
C₂₀H₁₈F₄O₅S

: 98-59-9
p-toluenesulfonyl chloride

: 1100362-45-5
C₂₇H₂₄F₄O₇S₂

Guidance literature:: C₂₀H₁₈F₄O₅S; p-toluenesulfonyl chloride; With triethylamine; In dichloromethane; at 20 ℃; for 6h;

With dmap; In dichloromethane; for 14h;

Reference yield:

: 1100362-34-2
C₁₆H₁₃F₅O₂S

: 1100362-45-5
C₂₇H₂₄F₄O₇S₂

Guidance literature:: Multi-step reaction with 9 steps

1: potassium tert-butylate / tetrahydrofuran

2: Dess-Martin periodane / dichloromethane

3: trimethylsilyl trifluoromethanesulfonate

4: 3-chloro-benzenecarboperoxoic acid / dichloromethane

5: boron trifluoride diethyl etherate / dichloromethane

6: triethylamine / dichloromethane

7: potassium tert-butylate / tetrahydrofuran

8: ozone / dichloromethane

9: triethylamine

With trimethylsilyl trifluoromethanesulfonate; boron trifluoride diethyl etherate; potassium tert-butylate; Dess-Martin periodane; ozone; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmcl.2012.11.047

Reference yield:

: 944950-33-8
2-(2,3,6-trifluoro-benzylidene)-malonic acid dimethyl ester

: 1100362-45-5
C₂₇H₂₄F₄O₇S₂

Guidance literature:: Multi-step reaction with 11 steps

1: potassium carbonate / tetrahydrofuran

2: lithium aluminium tetrahydride / tetrahydrofuran

3: potassium tert-butylate / tetrahydrofuran

4: Dess-Martin periodane / dichloromethane

5: trimethylsilyl trifluoromethanesulfonate

6: 3-chloro-benzenecarboperoxoic acid / dichloromethane

7: boron trifluoride diethyl etherate / dichloromethane

8: triethylamine / dichloromethane

9: potassium tert-butylate / tetrahydrofuran

10: ozone / dichloromethane

11: triethylamine

With lithium aluminium tetrahydride; trimethylsilyl trifluoromethanesulfonate; boron trifluoride diethyl etherate; potassium tert-butylate; potassium carbonate; Dess-Martin periodane; ozone; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; 1: |Michael Addition;
DOI:10.1016/j.bmcl.2012.11.047