2-<(cyanoacetyl)amino>-5-<3-(N-methyl-N-benzylamino)-2-hydroxypropoxy>benzaldehyde ethylene acetal

Base Information

Chemical Name:2-<(cyanoacetyl)amino>-5-<3-(N-methyl-N-benzylamino)-2-hydroxypropoxy>benzaldehyde ethylene acetal
CAS No.:143268-78-4
Molecular Formula:C₂₃H₂₇N₃O₅
Molecular Weight:425.484
Hs Code.:

Synonyms:2-<(cyanoacetyl)amino>-5-<3-(N-methyl-N-benzylamino)-2-hydroxypropoxy>benzaldehyde ethylene acetal

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Chemical Property of 2-<(cyanoacetyl)amino>-5-<3-(N-methyl-N-benzylamino)-2-hydroxypropoxy>benzaldehyde ethylene acetal

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Technology Process of 2-<(cyanoacetyl)amino>-5-<3-(N-methyl-N-benzylamino)-2-hydroxypropoxy>benzaldehyde ethylene acetal

There total 4 articles about 2-<(cyanoacetyl)amino>-5-<3-(N-methyl-N-benzylamino)-2-hydroxypropoxy>benzaldehyde ethylene acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.9%

: 143268-77-3
2-<(cyanoacetyl)amino>-5-(2,3-epoxypropoxy)benzaldehyde ethylene acetal

: 103-67-3
benzyl-methyl-amine

: 143268-78-4
2-<(cyanoacetyl)amino>-5-<3-(N-methyl-N-benzylamino)-2-hydroxypropoxy>benzaldehyde ethylene acetal

Guidance literature:: In methanol; for 3h; Heating;
DOI:10.1021/jm00098a003

Reference yield:

: 98454-56-9
5-hydroxy-2-nitrobenzaldehyde ethylene acetal

: 143268-78-4
2-<(cyanoacetyl)amino>-5-<3-(N-methyl-N-benzylamino)-2-hydroxypropoxy>benzaldehyde ethylene acetal

Guidance literature:: Multi-step reaction with 4 steps

1: 59.9 percent / K₂CO₃ / methanol / 20 h / Heating

2: H₂ / 5percent Pd/C / ethyl acetate / 760 Torr / Ambient temperature

3: Et₃N / ethyl acetate / 0 °C

4: 78.9 percent / methanol / 3 h / Heating

With hydrogen; potassium carbonate; triethylamine; palladium on activated charcoal; In methanol; ethyl acetate;
DOI:10.1021/jm00098a003

Reference yield:

: 112859-49-1
5-(2,3-epoxypropoxy)-2-nitrobenzaldehyde ethylene acetal

: 143268-78-4
2-<(cyanoacetyl)amino>-5-<3-(N-methyl-N-benzylamino)-2-hydroxypropoxy>benzaldehyde ethylene acetal

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / 5percent Pd/C / ethyl acetate / 760 Torr / Ambient temperature

2: Et₃N / ethyl acetate / 0 °C

3: 78.9 percent / methanol / 3 h / Heating

With hydrogen; triethylamine; palladium on activated charcoal; In methanol; ethyl acetate;
DOI:10.1021/jm00098a003