(2-(4-fluorophenyl)-2-hydroxy-1-(3-trifluoromethyl)phenyl)ethanone O-benzyl oxime

Base Information

Chemical Name:(2-(4-fluorophenyl)-2-hydroxy-1-(3-trifluoromethyl)phenyl)ethanone O-benzyl oxime
CAS No.:1609285-12-2
Molecular Formula:C₂₂H₁₇F₄NO₂
Molecular Weight:403.376
Hs Code.:

Synonyms:(2-(4-fluorophenyl)-2-hydroxy-1-(3-trifluoromethyl)phenyl)ethanone O-benzyl oxime

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Chemical Property of (2-(4-fluorophenyl)-2-hydroxy-1-(3-trifluoromethyl)phenyl)ethanone O-benzyl oxime

Chemical Property:

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Technology Process of (2-(4-fluorophenyl)-2-hydroxy-1-(3-trifluoromethyl)phenyl)ethanone O-benzyl oxime

There total 4 articles about (2-(4-fluorophenyl)-2-hydroxy-1-(3-trifluoromethyl)phenyl)ethanone O-benzyl oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1609285-11-1
2-(4-fluorophenyl)-2-hydroxy-1-(3-(trifluoromethyl)phenyl)ethanone

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: 1609285-12-2
(2-(4-fluorophenyl)-2-hydroxy-1-(3-trifluoromethyl)phenyl)ethanone O-benzyl oxime

Guidance literature:: With sodium acetate; In tetrahydrofuran; water; for 12h; Reflux;

Reference yield:

: 57009-80-0
2-(3-(trifluoromethyl)phenyl)-1,3-dithiane

: 1609285-12-2
(2-(4-fluorophenyl)-2-hydroxy-1-(3-trifluoromethyl)phenyl)ethanone O-benzyl oxime

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 °C

1.2: 1 h / -78 - 20 °C

2.1: [bis-(trifluoroacetoxy)iodo]benzene / water; acetonitrile / 1 h / 20 °C

3.1: sodium acetate / tetrahydrofuran; water / 12 h / Reflux

With n-butyllithium; [bis-(trifluoroacetoxy)iodo]benzene; sodium acetate; In tetrahydrofuran; hexane; water; acetonitrile;

Reference yield:

: 1609285-10-0
(4-fluorophenyl)(2-(3-(trifluoromethyl)phenyl)-1,3-dithian-2-yl)methanol

: 1609285-12-2
(2-(4-fluorophenyl)-2-hydroxy-1-(3-trifluoromethyl)phenyl)ethanone O-benzyl oxime

Guidance literature:: Multi-step reaction with 2 steps

1: [bis-(trifluoroacetoxy)iodo]benzene / water; acetonitrile / 1 h / 20 °C

2: sodium acetate / tetrahydrofuran; water / 12 h / Reflux

With [bis-(trifluoroacetoxy)iodo]benzene; sodium acetate; In tetrahydrofuran; water; acetonitrile;