C₄₂H₆₀N₁₀O₉

Base Information

• Chemical Name: C₄₂H₆₀N₁₀O₉
• CAS No.: 1414689-52-3
• Molecular Formula: C₄₂H₆₀N₁₀O₉
• Molecular Weight: 849
• Mol file: 1414689-52-3.mol

Synonyms:C₄₂H₆₀N₁₀O₉

Chemical Property of C₄₂H₆₀N₁₀O₉

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₂H₆₀N₁₀O₉

There total 5 articles about C₄₂H₆₀N₁₀O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

2,2',2''-triaminotriethylamine (4097-89-6) + C12H14N2O3 (1414689-37-4) → C42H60N10O9 (1414689-52-3)

Guidance literature:

In dichloromethane; at 0 ℃; for 0.333333h; Inert atmosphere; Reflux;

DOI:10.1016/j.tetlet.2012.09.025

Reference yield:

C11H16N2O2*C2HF3O2 (1414689-21-6) → C42H60N10O9 (1414689-52-3)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium hydrogencarbonate / dichloromethane / 0.01 h

1.2: 0.33 h

2.1: dichloromethane / 0.33 h / 0 °C / Inert atmosphere; Reflux

With sodium hydrogencarbonate; In dichloromethane;

DOI:10.1016/j.tetlet.2012.09.025

Reference yield:

benzyl 3-(t-butoxycarbonylamino)propanohydroxamate (136413-17-7) → C42H60N10O9 (1414689-52-3)

Guidance literature:

Multi-step reaction with 4 steps

1.1: potassium carbonate / acetonitrile / 40 °C

2.1: dichloromethane / 20 °C

3.1: sodium hydrogencarbonate / dichloromethane / 0.01 h

3.2: 0.33 h

4.1: dichloromethane / 0.33 h / 0 °C / Inert atmosphere; Reflux

With sodium hydrogencarbonate; potassium carbonate; In dichloromethane; acetonitrile;

DOI:10.1016/j.tetlet.2012.09.025

upstream raw materials:

C₁₁H₁₆N₂O₂*C₂HF₃O₂

2,2',2''-triaminotriethylamine

C₁₂H₁₄N₂O₃

benzyl 3-(t-butoxycarbonylamino)propanohydroxamate