1-((S)-(1-hydroxymethyl-2-phenyl)ethyl)-1H-1,2,3-triazole-4-carboxylic acid methyl ester

Base Information

• Chemical Name: 1-((S)-(1-hydroxymethyl-2-phenyl)ethyl)-1H-1,2,3-triazole-4-carboxylic acid methyl ester
• CAS No.: 1260955-44-9
• Molecular Formula: C₁₃H₁₅N₃O₃
• Molecular Weight: 261.28

Synonyms:1-((S)-(1-hydroxymethyl-2-phenyl)ethyl)-1H-1,2,3-triazole-4-carboxylic acid methyl ester

Chemical Property of 1-((S)-(1-hydroxymethyl-2-phenyl)ethyl)-1H-1,2,3-triazole-4-carboxylic acid methyl ester

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Technology Process of 1-((S)-(1-hydroxymethyl-2-phenyl)ethyl)-1H-1,2,3-triazole-4-carboxylic acid methyl ester

There total 1 articles about 1-((S)-(1-hydroxymethyl-2-phenyl)ethyl)-1H-1,2,3-triazole-4-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

propynoic acid methyl ester (922-67-8) + (S)-2-azido-3-phenyl-propan-1-ol (439694-28-7) → 1-((S)-(1-hydroxymethyl-2-phenyl)ethyl)-1H-1,2,3-triazole-4-carboxylic acid methyl ester (1260955-44-9)

Guidance literature:

With copper(II) sulfate; sodium L-ascorbate; In water; tert-butyl alcohol; at 20 ℃; for 15h;

DOI:10.3390/molecules14125124

Reference yield: 97.0%

1-((S)-(1-hydroxymethyl-2-phenyl)ethyl)-1H-1,2,3-triazole-4-carboxylic acid methyl ester (1260955-44-9) → 1-((S)-1-benzyl-2-hydroxyethyl)-1H-1,2,3-triazole-4-carboxylic acid amide (1260955-38-1)

Guidance literature:

With ammonia; In methanol; at 20 ℃;

DOI:10.3390/molecules14125124

Reference yield: 58.0%

1-((S)-(1-hydroxymethyl-2-phenyl)ethyl)-1H-1,2,3-triazole-4-carboxylic acid methyl ester (1260955-44-9) + N-butylamine (109-73-9,85404-21-3) → 1-((S)-1-benzyl-2-hydroxyethyl)-1H-1,2,3-triazole-4-carboxylic acid butylamide (1260955-51-8)

Guidance literature:

1-((S)-(1-hydroxymethyl-2-phenyl)ethyl)-1H-1,2,3-triazole-4-carboxylic acid methyl ester; N-butylamine; With methanol; sodium; at 20 ℃; for 15h; Inert atmosphere;

With hydrogenchloride; water; In methanol;

DOI:10.3390/molecules14125124

upstream raw materials:

propynoic acid methyl ester

(S)-2-azido-3-phenyl-propan-1-ol

Downstream raw materials:

[1-((S)-1-benzyl-2-hydroxyethyl)-1H-1,2,3-triazol-4-yl]-morpholin-4-yl-methanone

1-((S)-1-benzyl-2-hydroxyethyl)-1H-1,2,3-triazole-4-carboxylic acid amide

1-((S)-1-benzyl-2-hydroxyethyl)-1H-1,2,3-triazole-4-carboxylic acid (2-hydroxy-ethyl)-amide

1-((S)-(1-hydroxymethyl-2-phenyl)ethyl)-1H-1,2,3-triazole-4-carboxylic acid diethylamide

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