3-phenyl-4-(trifluoromethyl)-5-(7-vinyl-4,5-dihydro-2H-benzo[g]indazol-3-yl)isoxazole

Base Information

Chemical Name:3-phenyl-4-(trifluoromethyl)-5-(7-vinyl-4,5-dihydro-2H-benzo[g]indazol-3-yl)isoxazole
CAS No.:1307812-79-8
Molecular Formula:C₂₃H₁₆F₃N₃O
Molecular Weight:407.395
Hs Code.:

Synonyms:3-phenyl-4-(trifluoromethyl)-5-(7-vinyl-4,5-dihydro-2H-benzo[g]indazol-3-yl)isoxazole

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Chemical Property of 3-phenyl-4-(trifluoromethyl)-5-(7-vinyl-4,5-dihydro-2H-benzo[g]indazol-3-yl)isoxazole

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Technology Process of 3-phenyl-4-(trifluoromethyl)-5-(7-vinyl-4,5-dihydro-2H-benzo[g]indazol-3-yl)isoxazole

There total 6 articles about 3-phenyl-4-(trifluoromethyl)-5-(7-vinyl-4,5-dihydro-2H-benzo[g]indazol-3-yl)isoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.6%

: 1307812-78-7
2-(3-phenyl-4-(trifluoromethyl)isoxazole-5-carbonyl)-6-vinyl-3,4-dihydronaphthalen-1(2H)-one

: 1307812-79-8
3-phenyl-4-(trifluoromethyl)-5-(7-vinyl-4,5-dihydro-2H-benzo[g]indazol-3-yl)isoxazole

Guidance literature:: With hydrazine hydrate; In 1,4-dioxane; methanol; at 20 - 90 ℃; for 15h;

Reference yield:

: 932-90-1,622-31-1,140461-24-1,140461-25-2,622-32-2
syn-benzaldehyde oxime

: 1307812-79-8
3-phenyl-4-(trifluoromethyl)-5-(7-vinyl-4,5-dihydro-2H-benzo[g]indazol-3-yl)isoxazole

Guidance literature:: Multi-step reaction with 6 steps

1.1: N-chloro-succinimide / N,N-dimethyl-formamide / 20 °C

2.1: triethylamine / 1,2-dichloro-ethane / 20 °C

3.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / acetonitrile / 35 °C / sodium phosphate buffer

3.2: 20 °C

4.1: pyridine / dichloromethane / 20 °C

5.1: lithium diisopropyl amide / tetrahydrofuran / 0.37 h / -78 °C

5.2: 0.53 h / -78 - 20 °C

6.1: hydrazine hydrate / 1,4-dioxane; methanol / 15 h / 20 - 90 °C

With pyridine; N-chloro-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; hydrazine hydrate; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 934-16-7
phenylhydroxamoyl chloride

: 1307812-79-8
3-phenyl-4-(trifluoromethyl)-5-(7-vinyl-4,5-dihydro-2H-benzo[g]indazol-3-yl)isoxazole

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine / 1,2-dichloro-ethane / 20 °C

2.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / acetonitrile / 35 °C / sodium phosphate buffer

2.2: 20 °C

3.1: pyridine / dichloromethane / 20 °C

4.1: lithium diisopropyl amide / tetrahydrofuran / 0.37 h / -78 °C

4.2: 0.53 h / -78 - 20 °C

5.1: hydrazine hydrate / 1,4-dioxane; methanol / 15 h / 20 - 90 °C

With pyridine; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; hydrazine hydrate; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; 1,2-dichloro-ethane; acetonitrile;