10,22-bis(p-tolylsulphonyl)-1,4,7,13,16,19-hexaoxa-10,22-diazcyclotetracosane

Base Information

Chemical Name:10,22-bis(p-tolylsulphonyl)-1,4,7,13,16,19-hexaoxa-10,22-diazcyclotetracosane
CAS No.:101210-59-7
Molecular Formula:C₃₀H₄₆N₂O₁₀S₂
Molecular Weight:658.835
Hs Code.:

Synonyms:10,22-bis(p-tolylsulphonyl)-1,4,7,13,16,19-hexaoxa-10,22-diazcyclotetracosane

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Chemical Property of 10,22-bis(p-tolylsulphonyl)-1,4,7,13,16,19-hexaoxa-10,22-diazcyclotetracosane

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Technology Process of 10,22-bis(p-tolylsulphonyl)-1,4,7,13,16,19-hexaoxa-10,22-diazcyclotetracosane

There total 4 articles about 10,22-bis(p-tolylsulphonyl)-1,4,7,13,16,19-hexaoxa-10,22-diazcyclotetracosane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 31255-26-2
1-bromo-2-{2-[2-(2-bromoethoxy)ethoxy]-ethoxy}ethane

: 59945-36-7
1,11-bis(p-tolylsulphonylamino)-3,6,9-trioxaundecane

: 101210-59-7
10,22-bis(p-tolylsulphonyl)-1,4,7,13,16,19-hexaoxa-10,22-diazcyclotetracosane

Guidance literature:: With sodium hydroxide; tetra-(n-butyl)ammonium iodide; In toluene; for 10h; Heating;

Reference yield: 10.0%

: 7146-67-0
N-tosyldiethanolamine

: 7460-82-4
diethylene glycol ditosylate

: 98572-17-9
N-(p-tolylsulphonyl)-1,4,7-trioxa-10-azacyclododecane

: 101210-59-7
10,22-bis(p-tolylsulphonyl)-1,4,7,13,16,19-hexaoxa-10,22-diazcyclotetracosane

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 48h;

Reference yield:

: 31255-26-2
1-bromo-2-{2-[2-(2-bromoethoxy)ethoxy]-ethoxy}ethane

: 101210-59-7
10,22-bis(p-tolylsulphonyl)-1,4,7,13,16,19-hexaoxa-10,22-diazcyclotetracosane

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / sodium carbonate / H₂O / 4 h / Heating

2: 50 percent / tetrabutylammonium iodide, sodium hydroxide (50 percent) / toluene; H₂O / 9 h / Heating

With sodium hydroxide; tetra-(n-butyl)ammonium iodide; sodium carbonate; In water; toluene;