1,4,7,13,16,19-Hexaoxa-10,22-diazacyclotetracosane

Base Information

• Chemical Name: 1,4,7,13,16,19-Hexaoxa-10,22-diazacyclotetracosane
• CAS No.: 31255-17-1
• Molecular Formula: C16H34N2O6
• Molecular Weight: 350.456
• Hs Code.: 2934999090
• European Community (EC) Number: 250-537-1
• DSSTox Substance ID: DTXSID20185186
• Nikkaji Number: J278.077A
• Wikidata: Q83056182
• Mol file: 31255-17-1.mol

Synonyms:1,4,7,13,16,19-Hexaoxa-10,22-diazacyclotetracosane;31255-17-1;EINECS 250-537-1;SCHEMBL11554769;DTXSID20185186;STPLRJHSPOESPN-UHFFFAOYSA-N;C16H34N2O6;C16-H34-N2-O6;SR-01000390003;SR-01000390003-1;1,7,10,13,19,22 Hexaoxa-4,16-diazacyclotetracosane;1,7,10,13,19,22-Hexaoxa-4,16-diazacyclotetracosane

Chemical Property of 1,4,7,13,16,19-Hexaoxa-10,22-diazacyclotetracosane

Chemical Property:

• Vapor Pressure: 1.4E-10mmHg at 25°C
• Boiling Point: 511.6°Cat760mmHg
• PKA: 8.99±0.20(Predicted)
• Flash Point: 216.6°C
• PSA: 79.44000
• Density: 0.962g/cm³
• LogP: -0.06360
• XLogP3: -1.7
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 8
• Rotatable Bond Count: 0
• Exact Mass: 350.24168681
• Heavy Atom Count: 24
• Complexity: 205

Purity/Quality:

98%Min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1COCCOCCOCCNCCOCCOCCOCCN1

Technology Process of 1,4,7,13,16,19-Hexaoxa-10,22-diazacyclotetracosane

There total 7 articles about 1,4,7,13,16,19-Hexaoxa-10,22-diazacyclotetracosane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

→ 4,16-diaza-24-crown-8 (31255-17-1)

Guidance literature:

Reference yield: 47.0%

10,22-bis(p-tolylsulphonyl)-1,4,7,13,16,19-hexaoxa-10,22-diazcyclotetracosane (101210-59-7) → 4,16-diaza-24-crown-8 (31255-17-1)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 20h; Heating;

Reference yield: 14.0%

2-[2-[2-[2-aminoethoxy]ethoxy]ethoxy]ethylamine (929-75-9,892154-56-2) + 1,11-diiodo-3,6-9-trioxaundecane (36839-56-2) → 4,16-diaza-24-crown-8 (31255-17-1)

Guidance literature:

With potassium carbonate; In acetonitrile; for 168h; Heating;

upstream raw materials:

1,4,7,13,16,19-hexaoxa-10,22-diaza-cyclotetracosane-9,23-dione

10,22-bis(p-tolylsulphonyl)-1,4,7,13,16,19-hexaoxa-10,22-diazcyclotetracosane

2-[2-[2-[2-aminoethoxy]ethoxy]ethoxy]ethylamine

1,11-diiodo-3,6-9-trioxaundecane