(S)-2-(1,3-dioxoisoindolin-2-yl)-3-methyl-N-(2,4,6-trimethylbenzoyloxy)butanamide

Base Information

Chemical Name:(S)-2-(1,3-dioxoisoindolin-2-yl)-3-methyl-N-(2,4,6-trimethylbenzoyloxy)butanamide
CAS No.:1352720-50-3
Molecular Formula:C₂₃H₂₄N₂O₅
Molecular Weight:408.454
Hs Code.:

Synonyms:(S)-2-(1,3-dioxoisoindolin-2-yl)-3-methyl-N-(2,4,6-trimethylbenzoyloxy)butanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-(1,3-dioxoisoindolin-2-yl)-3-methyl-N-(2,4,6-trimethylbenzoyloxy)butanamide

Chemical Property:

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Technology Process of (S)-2-(1,3-dioxoisoindolin-2-yl)-3-methyl-N-(2,4,6-trimethylbenzoyloxy)butanamide

There total 4 articles about (S)-2-(1,3-dioxoisoindolin-2-yl)-3-methyl-N-(2,4,6-trimethylbenzoyloxy)butanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: O-(2,4,6-trimethylbenzoyl)hydroxylammonium chloride

: 6306-54-3
N-phthaloyl L-valine

: 1352720-50-3
(S)-2-(1,3-dioxoisoindolin-2-yl)-3-methyl-N-(2,4,6-trimethylbenzoyloxy)butanamide

Guidance literature:: N-phthaloyl L-valine; With 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride; In dichloromethane; at 0 ℃; for 10h; Inert atmosphere;

O-(2,4,6-trimethylbenzoyl)hydroxylammonium chloride; With 4-methyl-morpholine; In dichloromethane; at 0 - 20 ℃; for 10h; Inert atmosphere;
DOI:10.1002/anie.201103293

Reference yield:

: 162811-15-6
C₁₃H₁₄N₂O₄

: 938-18-1
mesitylene-2-carboxylic acid chloride

: 1352720-50-3
(S)-2-(1,3-dioxoisoindolin-2-yl)-3-methyl-N-(2,4,6-trimethylbenzoyloxy)butanamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃;
DOI:10.1002/anie.201103293

Reference yield:

: 5511-73-9
N-phthalimide l-valinyl chloride

: 1352720-50-3
(S)-2-(1,3-dioxoisoindolin-2-yl)-3-methyl-N-(2,4,6-trimethylbenzoyloxy)butanamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydroxylamine hydrochloride; sodium carbonate / diethyl ether; water / Inert atmosphere

2: triethylamine / dichloromethane / 0 °C

With hydroxylamine hydrochloride; sodium carbonate; triethylamine; In diethyl ether; dichloromethane; water;
DOI:10.1002/anie.201103293