3-benzyloxy-1-(1,3-bis(2-benzyloxy-1-benzyloxymethyl-ethoxy)-prop-2-yl)-6-methyl-4-(4-nitrophenyloxycarbonyl)-2-oxo-1,2-dihydropyridine

Base Information

• Chemical Name: 3-benzyloxy-1-(1,3-bis(2-benzyloxy-1-benzyloxymethyl-ethoxy)-prop-2-yl)-6-methyl-4-(4-nitrophenyloxycarbonyl)-2-oxo-1,2-dihydropyridine
• CAS No.: 872462-86-7
• Molecular Formula: C₅₇H₅₈N₂O₁₂
• Molecular Weight: 963.094

Synonyms:3-benzyloxy-1-(1,3-bis(2-benzyloxy-1-benzyloxymethyl-ethoxy)-prop-2-yl)-6-methyl-4-(4-nitrophenyloxycarbonyl)-2-oxo-1,2-dihydropyridine

Chemical Property of 3-benzyloxy-1-(1,3-bis(2-benzyloxy-1-benzyloxymethyl-ethoxy)-prop-2-yl)-6-methyl-4-(4-nitrophenyloxycarbonyl)-2-oxo-1,2-dihydropyridine

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Technology Process of 3-benzyloxy-1-(1,3-bis(2-benzyloxy-1-benzyloxymethyl-ethoxy)-prop-2-yl)-6-methyl-4-(4-nitrophenyloxycarbonyl)-2-oxo-1,2-dihydropyridine

There total 1 articles about 3-benzyloxy-1-(1,3-bis(2-benzyloxy-1-benzyloxymethyl-ethoxy)-prop-2-yl)-6-methyl-4-(4-nitrophenyloxycarbonyl)-2-oxo-1,2-dihydropyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) + 3-Benzyloxy-1-[1,3-bis-(2-benzyloxy-1-benzyloxymethyl-ethoxy)-prop-2-yl]-6-methyl-2-oxo-1,2-dihydropyridine-4-carboxylic acid (872462-85-6) → 3-benzyloxy-1-(1,3-bis(2-benzyloxy-1-benzyloxymethyl-ethoxy)-prop-2-yl)-6-methyl-4-(4-nitrophenyloxycarbonyl)-2-oxo-1,2-dihydropyridine (872462-86-7)

Guidance literature:

With dicyclohexyl-carbodiimide; In tetrahydrofuran; at 20 ℃; for 20h;

Reference yield: 83.0%

3-benzyloxy-1-(1,3-bis(2-benzyloxy-1-benzyloxymethyl-ethoxy)-prop-2-yl)-6-methyl-4-(4-nitrophenyloxycarbonyl)-2-oxo-1,2-dihydropyridine (872462-86-7) + 4-amino-5-[bis(2-aminoethyl)amino]pentanecarboxylic acid (872462-34-5) → 5-(bis-{2-[(3-benzyloxy-1-{[1,3-bis-(2-benzyloxy-1-benzyloxymethyl-ethoxy)-prop-2-yl]-carbamoyl}-6-methyl-2-oxo-1,2-dihydropyridine-4-carbonyl)-amino]ethyl}-amino)-4-[(3-benzyloxy-1-{[1,3-bis-(2-benzyloxy-1-benzyloxymethyl-ethoxy)-prop-2-yl]-carbamoyl}-6-methyl-2-oxo-1,2-dihydropyridine-4-carbonyl)-amino]-pentane carboxylic acid

Guidance literature:

In dichloromethane; at 20 ℃; for 72h;

Reference yield: 47.0%

4-amino-5-[bis(2-aminoethyl)amino]pentanecarboxylic acid (872463-07-5) + 3-benzyloxy-1-(1,3-bis(2-benzyloxy-1-benzyloxymethyl-ethoxy)-prop-2-yl)-6-methyl-4-(4-nitrophenyloxycarbonyl)-2-oxo-1,2-dihydropyridine (872462-86-7) → 4-(amino)-5-[bis(2-{3-benzyloxy-1-[1,3-bis(2-benzyloxy-1-benzyloxymethylethoxy)prop-2-yl]-6-methyl-2-oxo-1,2-dihydropyridine-4-carbonyl}aminoethyl)amino]pentane carboxylic acid (872462-90-3)

Guidance literature:

In dichloromethane; at 20 ℃; for 72h;

upstream raw materials:

4-nitro-phenol

3-Benzyloxy-1-[1,3-bis-(2-benzyloxy-1-benzyloxymethyl-ethoxy)-prop-2-yl]-6-methyl-2-oxo-1,2-dihydropyridine-4-carboxylic acid

Downstream raw materials:

4-(amino)-5-[bis(2-{3-benzyloxy-1-[1,3-bis(2-benzyloxy-1-benzyloxymethylethoxy)prop-2-yl]-6-methyl-2-oxo-1,2-dihydropyridine-4-carbonyl}aminoethyl)amino]pentane carboxylic acid

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