2-phenyl-5,6,7,8-tetrahydroquinoline N-oxide

Base Information

Chemical Name:2-phenyl-5,6,7,8-tetrahydroquinoline N-oxide
CAS No.:92850-39-0
Molecular Formula:C₁₅H₁₅NO
Molecular Weight:225.29
Hs Code.:

Synonyms:2-phenyl-5,6,7,8-tetrahydroquinoline N-oxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-phenyl-5,6,7,8-tetrahydroquinoline N-oxide

Chemical Property:

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Technology Process of 2-phenyl-5,6,7,8-tetrahydroquinoline N-oxide

There total 9 articles about 2-phenyl-5,6,7,8-tetrahydroquinoline N-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1570-04-3
2-phenyl-5,6,7,8-tetrahydroquinoline

: 92850-39-0
2-phenyl-5,6,7,8-tetrahydroquinoline N-oxide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 20 ℃;
DOI:10.1002/anie.200601529

Reference yield:

: 24740-01-0
2-(2-benzoylethyl)cyclohexanone

: 92850-39-0
2-phenyl-5,6,7,8-tetrahydroquinoline N-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: hydroxylamine hydrochloride / ethanol / 15 h / 85 °C

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / Reflux

With hydroxylamine hydrochloride; 3-chloro-benzenecarboperoxoic acid; In ethanol; dichloromethane;
DOI:10.1002/hlca.202000181

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 92850-39-0
2-phenyl-5,6,7,8-tetrahydroquinoline N-oxide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / diethyl ether / 4 h / 145 °C

2: hydroxylamine hydrochloride / ethanol / 15 h / 85 °C

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / Reflux

With hydroxylamine hydrochloride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; ethanol; dichloromethane;
DOI:10.1002/hlca.202000181