Technology Process of C36H38O6
There total 9 articles about C36H38O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 73 percent / NaIO4; aq. NaHCO3 / CH2Cl2 / 2 h / 20 °C
2: 59 percent / CuBr-Me2S / tetrahydrofuran; various solvent(s) / 2 h / -40 - 20 °C
3: 95 percent / NaH / dimethylformamide
4: 92 percent / 80 percent AcOH / 48 h / 70 °C
5: 68 percent / n-BuLi / diethyl ether / 20 °C
6: 85 percent / Cl2(PCy3)2Ru=CHPh / CH2Cl2 / 1 h / 20 °C
7: 92 percent / NaH / dimethylformamide
With
sodium periodate; n-butyllithium; sodium hydride; sodium hydrogencarbonate; acetic acid;
Grubbs catalyst first generation;
In
tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
5: Wittig methylenation;
DOI:10.1016/S0040-4039(01)01946-3
- Guidance literature:
-
Multi-step reaction with 9 steps
1: 89 percent / NaH / dimethylformamide
2: 95 percent / 60 percent aq. AcOH / 20 °C
3: 73 percent / NaIO4; aq. NaHCO3 / CH2Cl2 / 2 h / 20 °C
4: 59 percent / CuBr-Me2S / tetrahydrofuran; various solvent(s) / 2 h / -40 - 20 °C
5: 95 percent / NaH / dimethylformamide
6: 92 percent / 80 percent AcOH / 48 h / 70 °C
7: 68 percent / n-BuLi / diethyl ether / 20 °C
8: 85 percent / Cl2(PCy3)2Ru=CHPh / CH2Cl2 / 1 h / 20 °C
9: 92 percent / NaH / dimethylformamide
With
sodium periodate; n-butyllithium; sodium hydride; sodium hydrogencarbonate; acetic acid;
Grubbs catalyst first generation;
In
tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
7: Wittig methylenation;
DOI:10.1016/S0040-4039(01)01946-3