N-<5-(benzyloxycarbonyl-O-benzyl-L-tyrosyl)aminovaleryl>-N,N'-dicyclohexylurea

Base Information

Chemical Name:N-<5-(benzyloxycarbonyl-O-benzyl-L-tyrosyl)aminovaleryl>-N,N'-dicyclohexylurea
CAS No.:80977-30-6
Molecular Formula:C₄₂H₅₄N₄O₆
Molecular Weight:710.914
Hs Code.:

Synonyms:N-<5-(benzyloxycarbonyl-O-benzyl-L-tyrosyl)aminovaleryl>-N,N'-dicyclohexylurea

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Chemical Property of N-<5-(benzyloxycarbonyl-O-benzyl-L-tyrosyl)aminovaleryl>-N,N'-dicyclohexylurea

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Technology Process of N-<5-(benzyloxycarbonyl-O-benzyl-L-tyrosyl)aminovaleryl>-N,N'-dicyclohexylurea

There total 5 articles about N-<5-(benzyloxycarbonyl-O-benzyl-L-tyrosyl)aminovaleryl>-N,N'-dicyclohexylurea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 80977-28-2
5-(benzyloxycarbonyl-O-benzyl-L-tyrosyl)aminovaleric acid

: 2387-23-7
1,3-Dicyclohexylurea

: 80977-29-3
[(S)-1-(4-Benzyloxy-benzyl)-2-oxo-2-(2-oxo-piperidin-1-yl)-ethyl]-carbamic acid benzyl ester

: 80977-30-6
N-<5-(benzyloxycarbonyl-O-benzyl-L-tyrosyl)aminovaleryl>-N,N'-dicyclohexylurea

Guidance literature:: With dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; for 12h; Ambient temperature;
DOI:10.1071/CH9812439

Reference yield: 41.0%

: 80977-28-2
5-(benzyloxycarbonyl-O-benzyl-L-tyrosyl)aminovaleric acid

: 538-75-0
dicyclohexyl-carbodiimide

: 2387-23-7
1,3-Dicyclohexylurea

: 80977-29-3
[(S)-1-(4-Benzyloxy-benzyl)-2-oxo-2-(2-oxo-piperidin-1-yl)-ethyl]-carbamic acid benzyl ester

: 80977-30-6
N-<5-(benzyloxycarbonyl-O-benzyl-L-tyrosyl)aminovaleryl>-N,N'-dicyclohexylurea

Guidance literature:: In N,N-dimethyl-formamide; for 12h; Ambient temperature;
DOI:10.1071/CH9812439

Reference yield:

: 3562-03-6
Z-Tyr(OBzl)-ONp

: 80977-30-6
N-<5-(benzyloxycarbonyl-O-benzyl-L-tyrosyl)aminovaleryl>-N,N'-dicyclohexylurea

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / N-methylmorpholine / dimethylformamide

2: 91 percent / CF₃COOH, anisole

3: 45 percent / N,N'-dicyclohexylcarbodiimide / dimethylformamide / 12 h / Ambient temperature

With 4-methyl-morpholine; methoxybenzene; dicyclohexyl-carbodiimide; trifluoroacetic acid; In N,N-dimethyl-formamide;
DOI:10.1071/CH9812439