butane-1,1,3-triyltribenzene

Base Information

Chemical Name:butane-1,1,3-triyltribenzene
CAS No.:110747-03-0
Molecular Formula:C₂₂H₂₂
Molecular Weight:286.417
Hs Code.:

Synonyms:butane-1,1,3-triyltribenzene

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Chemical Property of butane-1,1,3-triyltribenzene

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Technology Process of butane-1,1,3-triyltribenzene

There total 7 articles about butane-1,1,3-triyltribenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 530-48-3
1,1-Diphenylethylene

: di-tert-butyl 2,6-dimethyl-4-(1-phenylethyl)-1,4-dihydropyridine-3,5-dicarboxylate

: 110747-03-0
butane-1,1,3-triyltribenzene

Guidance literature:: With tris[2-phenylpyridinato-C²,N]iridium(III); In N,N-dimethyl-formamide; at 20 ℃; for 48h; Inert atmosphere; Irradiation;
DOI:10.1002/adsc.201701348

Reference yield:

: 34713-70-7
2-Phenylpropanal

: 110747-03-0
butane-1,1,3-triyltribenzene

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium hydroxide / ethanol / 12 h / 90 °C / Inert atmosphere

2: tris[2-phenylpyridinato-C²,N]iridium(III) / N,N-dimethyl-formamide / 48 h / 20 °C / Inert atmosphere; Irradiation

With ammonium hydroxide; tris[2-phenylpyridinato-C²,N]iridium(III); In ethanol; N,N-dimethyl-formamide; 2: |Michael Addition;
DOI:10.1002/adsc.201701348