2-methoxy-8,9-dihydro-7H-benzocyclohepten-6-yl nonafluorobutane-1-sulphonate

Base Information

Chemical Name:2-methoxy-8,9-dihydro-7H-benzocyclohepten-6-yl nonafluorobutane-1-sulphonate
CAS No.:1143510-06-8
Molecular Formula:C₁₆H₁₃F₉O₄S
Molecular Weight:472.328
Hs Code.:

Synonyms:2-methoxy-8,9-dihydro-7H-benzocyclohepten-6-yl nonafluorobutane-1-sulphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-methoxy-8,9-dihydro-7H-benzocyclohepten-6-yl nonafluorobutane-1-sulphonate

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Technology Process of 2-methoxy-8,9-dihydro-7H-benzocyclohepten-6-yl nonafluorobutane-1-sulphonate

There total 1 articles about 2-methoxy-8,9-dihydro-7H-benzocyclohepten-6-yl nonafluorobutane-1-sulphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 375-72-4
Nonafluorobutanesulfonyl fluoride

: 1143510-32-0
5-(2-benzyloxyethyl)-2-methoxy-5,7,8,9-tetrahydrobenzocyclohepten-6-one

: 40463-28-3
2-methoxy-5,7,8,9-tetrahydrobenzocyclohepten-6-one

: 1143510-06-8
2-methoxy-8,9-dihydro-7H-benzocyclohepten-6-yl nonafluorobutane-1-sulphonate

: 1143510-33-1
5-(2-benzyloxyethyl)-2-methoxy-8,9-dihydro-7H-benzocyclohepten-6-yl nonafluorobutane-1-sulphonate

Guidance literature:: 5-(2-benzyloxyethyl)-2-methoxy-5,7,8,9-tetrahydrobenzocyclohepten-6-one; 2-methoxy-5,7,8,9-tetrahydrobenzocyclohepten-6-one; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In toluene; at 0 ℃; for 0.25h;

Nonafluorobutanesulfonyl fluoride; In toluene; at 20 ℃; for 0.333333h;

Reference yield:

: 1143510-06-8
2-methoxy-8,9-dihydro-7H-benzocyclohepten-6-yl nonafluorobutane-1-sulphonate

: 1143510-33-1
5-(2-benzyloxyethyl)-2-methoxy-8,9-dihydro-7H-benzocyclohepten-6-yl nonafluorobutane-1-sulphonate

: 5720-07-0
4-methoxyphenylboronic acid

: 1143510-34-2
9-(2-benzyloxyethyl)-3-methoxy-8-(4-methoxyphenyl)-6,7-dihydro-5H-benzocycloheptene

: 3-methoxy-8-(4-methoxyphenyl)-6,7-dihydro-5H-benzocycloheptene

Guidance literature:: With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; water; toluene; at 120 ℃; for 1h; microwave irradiation;