2-[2-(5-tert-butyl-2-methylphenyl)-3,3,4,4,5,5-hexafluorocyclopent-1-enyl]-3,5-dimethylthiophene

Base Information

Chemical Name:2-[2-(5-tert-butyl-2-methylphenyl)-3,3,4,4,5,5-hexafluorocyclopent-1-enyl]-3,5-dimethylthiophene
CAS No.:1201171-90-5
Molecular Formula:C₂₂H₂₂F₆S
Molecular Weight:432.473
Hs Code.:

Synonyms:2-[2-(5-tert-butyl-2-methylphenyl)-3,3,4,4,5,5-hexafluorocyclopent-1-enyl]-3,5-dimethylthiophene

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Chemical Property of 2-[2-(5-tert-butyl-2-methylphenyl)-3,3,4,4,5,5-hexafluorocyclopent-1-enyl]-3,5-dimethylthiophene

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Technology Process of 2-[2-(5-tert-butyl-2-methylphenyl)-3,3,4,4,5,5-hexafluorocyclopent-1-enyl]-3,5-dimethylthiophene

There total 2 articles about 2-[2-(5-tert-butyl-2-methylphenyl)-3,3,4,4,5,5-hexafluorocyclopent-1-enyl]-3,5-dimethylthiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.9%

: 61024-94-0
2-bromo-4-tert-butyl-1-methylbenzene

: 173345-48-7
2-(2,3,3,4,4,5,5-heptafluorocyclopent-1-en-1-yl)-3,5-dimethylthiophene

: 1201171-90-5
2-[2-(5-tert-butyl-2-methylphenyl)-3,3,4,4,5,5-hexafluorocyclopent-1-enyl]-3,5-dimethylthiophene

Guidance literature:: 2-bromo-4-tert-butyl-1-methylbenzene; With n-butyllithium; In tetrahydrofuran; hexane; at -70 ℃; for 0.5h; Inert atmosphere;

2-(2,3,3,4,4,5,5-heptafluorocyclopent-1-en-1-yl)-3,5-dimethylthiophene; In tetrahydrofuran; hexane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1246/cl.2009.982

Reference yield:

: C₂₂H₂₂F₆S

: 1201171-90-5
2-[2-(5-tert-butyl-2-methylphenyl)-3,3,4,4,5,5-hexafluorocyclopent-1-enyl]-3,5-dimethylthiophene

Guidance literature:: at 25 ℃; Activation energy;
DOI:10.1246/cl.2009.982

Reference yield:

: 1201171-90-5
2-[2-(5-tert-butyl-2-methylphenyl)-3,3,4,4,5,5-hexafluorocyclopent-1-enyl]-3,5-dimethylthiophene

: 1201171-93-8
2-[2-(5-tert-butyl-3-iodomethyl-2-methylphenyl)-3,3,4,4,5,5-hexafluorocyclopent-1-enyl]-4-iodomethyl-3,5-dimethylthiophene

Guidance literature:: Multi-step reaction with 2 steps

1: iron(III) chloride / dichloromethane / 1 h

2: sodium iodide / acetone / 0.5 h / Reflux

With iron(III) chloride; sodium iodide; In dichloromethane; acetone;
DOI:10.1246/cl.2009.982