6-formyl-5-phenyl-5-vinylhexanoic acid ethylene acetal

Base Information

Chemical Name:6-formyl-5-phenyl-5-vinylhexanoic acid ethylene acetal
CAS No.:134756-93-7
Molecular Formula:C₁₇H₂₂O₄
Molecular Weight:290.359
Hs Code.:

Synonyms:6-formyl-5-phenyl-5-vinylhexanoic acid ethylene acetal

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Chemical Property of 6-formyl-5-phenyl-5-vinylhexanoic acid ethylene acetal

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Technology Process of 6-formyl-5-phenyl-5-vinylhexanoic acid ethylene acetal

There total 6 articles about 6-formyl-5-phenyl-5-vinylhexanoic acid ethylene acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 5-[1,3]Dioxolan-2-ylmethyl-5-phenyl-hept-6-enenitrile

: 134756-93-7
6-formyl-5-phenyl-5-vinylhexanoic acid ethylene acetal

Guidance literature:: With potassium hydroxide; dihydrogen peroxide; 1.) 40 deg C, 1 h, 2.) 111 deg C, 3 h;
DOI:10.1021/ja00015a037

Reference yield:

: 108212-22-2
6-iodo-3-phenyl-3-vinylhexanal

: 134756-93-7
6-formyl-5-phenyl-5-vinylhexanoic acid ethylene acetal

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / p-toluenesulfonic acid / benzene / 12 h / Heating

2: 80 percent / dimethylsulfoxide / 3 h / 120 °C

3: 69 percent / 30percent aq. KOH, 30percent H₂O₂ / 1.) 40 deg C, 1 h, 2.) 111 deg C, 3 h

With potassium hydroxide; dihydrogen peroxide; toluene-4-sulfonic acid; In dimethyl sulfoxide; benzene;
DOI:10.1021/ja00015a037

Reference yield:

: 2-(5-Iodo-2-phenyl-2-vinyl-pentyl)-[1,3]dioxolane

: 134756-93-7
6-formyl-5-phenyl-5-vinylhexanoic acid ethylene acetal

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / dimethylsulfoxide / 3 h / 120 °C

2: 69 percent / 30percent aq. KOH, 30percent H₂O₂ / 1.) 40 deg C, 1 h, 2.) 111 deg C, 3 h

With potassium hydroxide; dihydrogen peroxide; In dimethyl sulfoxide;
DOI:10.1021/ja00015a037