3-(3-bromobenzyl)-1-(3,4-dimethoxybenzyl)-4-phenyl-1H-1,2,3-triazolium bromide

Base Information

Chemical Name:3-(3-bromobenzyl)-1-(3,4-dimethoxybenzyl)-4-phenyl-1H-1,2,3-triazolium bromide
CAS No.:1422251-42-0
Molecular Formula:Br*C₂₄H₂₃BrN₃O₂
Molecular Weight:545.274
Hs Code.:

Synonyms:3-(3-bromobenzyl)-1-(3,4-dimethoxybenzyl)-4-phenyl-1H-1,2,3-triazolium bromide

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Chemical Property of 3-(3-bromobenzyl)-1-(3,4-dimethoxybenzyl)-4-phenyl-1H-1,2,3-triazolium bromide

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Technology Process of 3-(3-bromobenzyl)-1-(3,4-dimethoxybenzyl)-4-phenyl-1H-1,2,3-triazolium bromide

There total 3 articles about 3-(3-bromobenzyl)-1-(3,4-dimethoxybenzyl)-4-phenyl-1H-1,2,3-triazolium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 823-78-9
meta-bromobenzyl bromide

: 1422251-43-1
1-(3,4-dimethoxybenzyl)-4-phenyl-1H-1,2,3-triazole

: 1422251-42-0
3-(3-bromobenzyl)-1-(3,4-dimethoxybenzyl)-4-phenyl-1H-1,2,3-triazolium bromide

Guidance literature:: In acetonitrile; at 80 ℃; for 11h;
DOI:10.1055/s-0032-1316806

Reference yield:

: 7306-46-9
4-chloromethyl-1,2-dimethoxy-benzene

: 1422251-42-0
3-(3-bromobenzyl)-1-(3,4-dimethoxybenzyl)-4-phenyl-1H-1,2,3-triazolium bromide

Guidance literature:: Multi-step reaction with 3 steps

1: water; sodium azide / tert-butyl alcohol / 24 h / 20 °C

2: sodium L-ascorbate; copper(II) sulfate / tert-butyl alcohol; water / 24 h / 20 °C

3: acetonitrile / 11 h / 80 °C

With sodium azide; water; copper(II) sulfate; sodium L-ascorbate; In water; acetonitrile; tert-butyl alcohol;
DOI:10.1055/s-0032-1316806

Reference yield:

: 90807-80-0
4-(azidomethyl)-1,2-dimethoxybenzene

: 1422251-42-0
3-(3-bromobenzyl)-1-(3,4-dimethoxybenzyl)-4-phenyl-1H-1,2,3-triazolium bromide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium L-ascorbate; copper(II) sulfate / tert-butyl alcohol; water / 24 h / 20 °C

2: acetonitrile / 11 h / 80 °C

With copper(II) sulfate; sodium L-ascorbate; In water; acetonitrile; tert-butyl alcohol;
DOI:10.1055/s-0032-1316806