(2S)-tert-butoxycarbonylamino-pentanedioic acid 1-benzyl ester 5-cyclohexyl ester

Base Information

Chemical Name:(2S)-tert-butoxycarbonylamino-pentanedioic acid 1-benzyl ester 5-cyclohexyl ester
CAS No.:73821-96-2
Molecular Formula:C₂₃H₃₃NO₆
Molecular Weight:419.518
Hs Code.:

Synonyms:(2S)-tert-butoxycarbonylamino-pentanedioic acid 1-benzyl ester 5-cyclohexyl ester

Suppliers and Price of (2S)-tert-butoxycarbonylamino-pentanedioic acid 1-benzyl ester 5-cyclohexyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (2S)-tert-butoxycarbonylamino-pentanedioic acid 1-benzyl ester 5-cyclohexyl ester

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of (2S)-tert-butoxycarbonylamino-pentanedioic acid 1-benzyl ester 5-cyclohexyl ester

There total 1 articles about (2S)-tert-butoxycarbonylamino-pentanedioic acid 1-benzyl ester 5-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 73821-97-3,133464-27-4
N-α-tert-butyloxycarbonyl-glutamic acid, γ-cyclohexyl ester

: 100-39-0
benzyl bromide

: 73821-96-2
(2S)-tert-butoxycarbonylamino-pentanedioic acid 1-benzyl ester 5-cyclohexyl ester

Guidance literature:: With caesium carbonate; In methanol;
DOI:10.1016/j.bmcl.2006.07.059

Reference yield: 96.0%

: 73821-96-2
(2S)-tert-butoxycarbonylamino-pentanedioic acid 1-benzyl ester 5-cyclohexyl ester

: 915194-00-2
(2S)-aminopentanedioic acid 1-benzyl ester 5-cyclohexyl ester

Guidance literature:: With sulfuric acid; In ethyl acetate;
DOI:10.1016/j.bmcl.2006.07.059

Reference yield:

: 73821-96-2
(2S)-tert-butoxycarbonylamino-pentanedioic acid 1-benzyl ester 5-cyclohexyl ester

: (S)-2-[4-((S)-1-Benzyloxycarbonyl-3-cyclohexyloxycarbonyl-propylamino)-butyrylamino]-pentanedioic acid dibenzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / H₂SO₄ / ethyl acetate

2: 43 percent / NaBH₃CN; AcOH / methanol / 20 °C

With sulfuric acid; sodium cyanoborohydride; acetic acid; In methanol; ethyl acetate;
DOI:10.1016/j.bmcl.2006.07.059