N-(Carbobenzyloxy)-L-alanine 9,10-dimethylanthracene acyl nitroso adduct

Base Information

Chemical Name:N-(Carbobenzyloxy)-L-alanine 9,10-dimethylanthracene acyl nitroso adduct
CAS No.:160057-14-7
Molecular Formula:C₂₇H₂₆N₂O₄
Molecular Weight:442.514
Hs Code.:

Synonyms:N-(Carbobenzyloxy)-L-alanine 9,10-dimethylanthracene acyl nitroso adduct

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Chemical Property of N-(Carbobenzyloxy)-L-alanine 9,10-dimethylanthracene acyl nitroso adduct

Chemical Property:

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Technology Process of N-(Carbobenzyloxy)-L-alanine 9,10-dimethylanthracene acyl nitroso adduct

There total 3 articles about N-(Carbobenzyloxy)-L-alanine 9,10-dimethylanthracene acyl nitroso adduct which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 781-43-1
9,10-dimethylanthracene

: 160056-97-3
(S)-Nα-(benzyloxycarbonyl)alanine hydroxamic acid

: 160057-14-7
N-(Carbobenzyloxy)-L-alanine 9,10-dimethylanthracene acyl nitroso adduct

Guidance literature:: With tetrabutylammonium periodite; In methanol; dichloromethane; for 1h;
DOI:10.1021/jo00095a040

Reference yield:

: 1142-20-7
N-Cbz-Ala

: 160057-14-7
N-(Carbobenzyloxy)-L-alanine 9,10-dimethylanthracene acyl nitroso adduct

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂

2: 96 percent / NH₂OH*HCl, KOH / methanol

3: 78 percent / tetra-n-butylammonium periodate / methanol; CH₂Cl₂ / 1 h

With potassium hydroxide; thionyl chloride; hydroxylamine hydrochloride; tetrabutylammonium periodite; In methanol; dichloromethane;
DOI:10.1021/jo00095a040

Reference yield:

: 28819-05-8
(S)-2-benzyloxycarbonylamino-propionic acid methyl ester

: 160057-14-7
N-(Carbobenzyloxy)-L-alanine 9,10-dimethylanthracene acyl nitroso adduct

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / NH₂OH*HCl, KOH / methanol

2: 78 percent / tetra-n-butylammonium periodate / methanol; CH₂Cl₂ / 1 h

With potassium hydroxide; hydroxylamine hydrochloride; tetrabutylammonium periodite; In methanol; dichloromethane;
DOI:10.1021/jo00095a040