(2-methyl-5-tert-butylphenyl) 3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:(2-methyl-5-tert-butylphenyl) 3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-1-thio-β-D-glucopyranoside
CAS No.:1529807-89-3
Molecular Formula:C₃₃H₃₆Cl₃NO₅S
Molecular Weight:665.078
Hs Code.:

Synonyms:(2-methyl-5-tert-butylphenyl) 3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-1-thio-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2-methyl-5-tert-butylphenyl) 3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-1-thio-β-D-glucopyranoside

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Technology Process of (2-methyl-5-tert-butylphenyl) 3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-1-thio-β-D-glucopyranoside

There total 3 articles about (2-methyl-5-tert-butylphenyl) 3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1529807-66-6
(2-methyl-5-tert-butylphenyl) 2-deoxy-2-trichloroacetamido-3,4,6-tri-O-trimethylsilyl-1-thio-β-D-glucopyranoside

: 100-52-7
benzaldehyde

: 1529807-89-3
(2-methyl-5-tert-butylphenyl) 3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-1-thio-β-D-glucopyranoside

Guidance literature:: With triethylsilane; trifluorormethanesulfonic acid; In dichloromethane; at 20 ℃; for 0.166667h; regioselective reaction; Molecular sieve; Inert atmosphere;
DOI:10.1039/c3cc48078j

Reference yield:

: 1529807-66-6
(2-methyl-5-tert-butylphenyl) 2-deoxy-2-trichloroacetamido-3,4,6-tri-O-trimethylsilyl-1-thio-β-D-glucopyranoside

: 100-52-7
benzaldehyde

: 1529807-89-3
(2-methyl-5-tert-butylphenyl) 3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-1-thio-β-D-glucopyranoside

: 1529808-02-3
(2-methyl-5-tert-butylphenyl) 3,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-1-thio-β-D-glucopyranoside

Guidance literature:: With triethylsilane; trifluorormethanesulfonic acid; In dichloromethane; at 20 ℃; for 0.25h; Reagent/catalyst; Solvent; Time; regioselective reaction; Inert atmosphere;
DOI:10.1039/c3cc48078j

Reference yield:

: 1529807-69-9
C₁₉H₂₆Cl₃NO₅S

: 1529807-89-3
(2-methyl-5-tert-butylphenyl) 3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 2 h / 20 °C / Inert atmosphere

2: trifluorormethanesulfonic acid; triethylsilane / dichloromethane / 0.17 h / 20 °C / Molecular sieve; Inert atmosphere

With triethylsilane; trifluorormethanesulfonic acid; In dichloromethane;
DOI:10.1039/c3cc48078j