Technology Process of C63H71N3O9Si
There total 22 articles about C63H71N3O9Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide;
In
dichloromethane;
for 0.333333h;
Inert atmosphere;
DOI:10.1002/chem.201400046
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine; fluorosilicic acid / water; acetonitrile / 12.5 h / 20 - 65 °C
2: HATU; N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 20 °C / Inert atmosphere
3: 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate / dichloromethane / 0.33 h / Inert atmosphere
With
fluorosilicic acid; tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide; triethylamine; N-ethyl-N,N-diisopropylamine; HATU;
In
dichloromethane; water; acetonitrile;
DOI:10.1002/chem.201400046
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: dichloromethane; methanol; diethyl ether / 0.25 h / 0 - 20 °C / Inert atmosphere
2.1: sodium hydride / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere
2.2: 1.5 h / 20 °C / Inert atmosphere
3.1: methanol; lithium hydroxide monohydrate / tetrahydrofuran; water / 3 h / 20 °C
4.1: triethylamine; dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 20 °C / Inert atmosphere
5.1: methanol; lithium hydroxide monohydrate / tetrahydrofuran; water / 0.5 h / 20 °C
6.1: HATU; N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 20 °C / Inert atmosphere
7.1: 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate / dichloromethane / 0.33 h / Inert atmosphere
With
methanol; dmap; tetrapropylammonium perruthennate; lithium hydroxide monohydrate; sodium hydride; benzotriazol-1-ol; 4-methylmorpholine N-oxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; HATU;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; water;
DOI:10.1002/chem.201400046