Acetic acid (S)-3-benzyloxymethoxy-4-{(4S,6S)-6-[(4S,6R)-6-((2R,4S)-2-benzyloxymethoxy-4-hydroxy-hept-6-enyl)-2,2-dimethyl-[1,3]dioxan-4-ylmethyl]-2,2-dimethyl-[1,3]dioxan-4-yl}-butyl ester

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Chemical Name:Acetic acid (S)-3-benzyloxymethoxy-4-{(4S,6S)-6-[(4S,6R)-6-((2R,4S)-2-benzyloxymethoxy-4-hydroxy-hept-6-enyl)-2,2-dimethyl-[1,3]dioxan-4-ylmethyl]-2,2-dimethyl-[1,3]dioxan-4-yl}-butyl ester
CAS No.:883554-55-0
Molecular Formula:C₄₂H₆₂O₁₁
Molecular Weight:742.948
Hs Code.:

Acetic acid (S)-3-benzyloxymethoxy-4-{(4S,6S)-6-[(4S,6R)-6-((2R,4S)-2-benzyloxymethoxy-4-hydroxy-hept-6-enyl)-2,2-dimethyl-[1,3]dioxan-4-ylmethyl]-2,2-dimethyl-[1,3]dioxan-4-yl}-butyl ester

Synonyms:Acetic acid (S)-3-benzyloxymethoxy-4-{(4S,6S)-6-[(4S,6R)-6-((2R,4S)-2-benzyloxymethoxy-4-hydroxy-hept-6-enyl)-2,2-dimethyl-[1,3]dioxan-4-ylmethyl]-2,2-dimethyl-[1,3]dioxan-4-yl}-butyl ester

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Chemical Property of Acetic acid (S)-3-benzyloxymethoxy-4-{(4S,6S)-6-[(4S,6R)-6-((2R,4S)-2-benzyloxymethoxy-4-hydroxy-hept-6-enyl)-2,2-dimethyl-[1,3]dioxan-4-ylmethyl]-2,2-dimethyl-[1,3]dioxan-4-yl}-butyl ester

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Technology Process of Acetic acid (S)-3-benzyloxymethoxy-4-{(4S,6S)-6-[(4S,6R)-6-((2R,4S)-2-benzyloxymethoxy-4-hydroxy-hept-6-enyl)-2,2-dimethyl-[1,3]dioxan-4-ylmethyl]-2,2-dimethyl-[1,3]dioxan-4-yl}-butyl ester

There total 5 articles about Acetic acid (S)-3-benzyloxymethoxy-4-{(4S,6S)-6-[(4S,6R)-6-((2R,4S)-2-benzyloxymethoxy-4-hydroxy-hept-6-enyl)-2,2-dimethyl-[1,3]dioxan-4-ylmethyl]-2,2-dimethyl-[1,3]dioxan-4-yl}-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 883554-54-9
Acetic acid (S)-4-((4S,6S)-6-{(4S,6R)-6-[(R)-4-(tert-butyl-dimethyl-silanyloxy)-2-hydroxy-butyl]-2,2-dimethyl-[1,3]dioxan-4-ylmethyl}-2,2-dimethyl-[1,3]dioxan-4-yl)-3-hydroxy-butyl ester

: 3587-60-8
Benzyloxymethyl chloride

: 883554-55-0
Acetic acid (S)-3-benzyloxymethoxy-4-{(4S,6S)-6-[(4S,6R)-6-((2R,4S)-2-benzyloxymethoxy-4-hydroxy-hept-6-enyl)-2,2-dimethyl-[1,3]dioxan-4-ylmethyl]-2,2-dimethyl-[1,3]dioxan-4-yl}-butyl ester

Guidance literature:: Multistep reaction;
DOI:10.1002/ejoc.200500670

Reference yield:

: 883554-50-5
(1S,6R)-6-hydroxy-4-{(2R,4S,6R)-2,4,8-trihydroxy-6-[(4-methoxybenzoyl)oxy]octyl}cyclohept-3-en-1-yl 4-methoxybenzoate

: 883554-55-0
Acetic acid (S)-3-benzyloxymethoxy-4-{(4S,6S)-6-[(4S,6R)-6-((2R,4S)-2-benzyloxymethoxy-4-hydroxy-hept-6-enyl)-2,2-dimethyl-[1,3]dioxan-4-ylmethyl]-2,2-dimethyl-[1,3]dioxan-4-yl}-butyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: imidazole / dimethylformamide / 0.75 h / 0 - 25 °C

1.2: 432 mg / camphorsulfonic acid / acetone / 0.33 h / 0 °C

2.1: NMO*H₂O; OsO₄ / H₂O; acetone / 1 h / 25 °C

2.2: NaIO₄ / dioxane; H₂O / 12 h / 25 °C

2.3: Et₂BOMe; NaBH₄ / tetrahydrofuran; methanol / 1 h / 25 °C

3.1: 530 mg / camphorsulfonic acid / acetone / 0.33 h / 0 °C

4.1: KOMe / methanol / 15 h / 0 - 25 °C

4.2: 79 percent / Candida cylindracea lipase / various solvent(s) / 1 h / 25 °C

With 1H-imidazole; osmium(VIII) oxide; camphor-10-sulfonic acid; potassium methanolate; 4-methylmorpholine N-oxide; In methanol; water; N,N-dimethyl-formamide; acetone;
DOI:10.1002/ejoc.200500670

Reference yield:

: 883554-51-6
(1S,6R)-6-hydroxy-4-{[(4R,6S)-6-{(2R)-2-(4-methoxybenzoyl)oxy}-4-{[tert-butyldimethylsilyloxy]butyl}-2,2-dimethyl-1,3-dioxan-4-yl]methyl}cyclohept-3-en-1-yl 4-methoxybenzoate

: 883554-55-0
Acetic acid (S)-3-benzyloxymethoxy-4-{(4S,6S)-6-[(4S,6R)-6-((2R,4S)-2-benzyloxymethoxy-4-hydroxy-hept-6-enyl)-2,2-dimethyl-[1,3]dioxan-4-ylmethyl]-2,2-dimethyl-[1,3]dioxan-4-yl}-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: NMO*H₂O; OsO₄ / H₂O; acetone / 1 h / 25 °C

1.2: NaIO₄ / dioxane; H₂O / 12 h / 25 °C

1.3: Et₂BOMe; NaBH₄ / tetrahydrofuran; methanol / 1 h / 25 °C

2.1: 530 mg / camphorsulfonic acid / acetone / 0.33 h / 0 °C

3.1: KOMe / methanol / 15 h / 0 - 25 °C

3.2: 79 percent / Candida cylindracea lipase / various solvent(s) / 1 h / 25 °C

With osmium(VIII) oxide; camphor-10-sulfonic acid; potassium methanolate; 4-methylmorpholine N-oxide; In methanol; water; acetone;
DOI:10.1002/ejoc.200500670