Acetic acid (S)-3-benzyloxymethoxy-4-((4S,6S)-6-{(4S,6R)-6-[(S)-2-benzyloxymethoxy-3-((4R,6R)-6-hydroxymethyl-2,2-dimethyl-[1,3]dioxan-4-yl)-propyl]-2,2-dimethyl-[1,3]dioxan-4-ylmethyl}-2,2-dimethyl-[1,3]dioxan-4-yl)-butyl ester

Base Information

Chemical Name:Acetic acid (S)-3-benzyloxymethoxy-4-((4S,6S)-6-{(4S,6R)-6-[(S)-2-benzyloxymethoxy-3-((4R,6R)-6-hydroxymethyl-2,2-dimethyl-[1,3]dioxan-4-yl)-propyl]-2,2-dimethyl-[1,3]dioxan-4-ylmethyl}-2,2-dimethyl-[1,3]dioxan-4-yl)-butyl ester
CAS No.:883554-57-2
Molecular Formula:C₄₅H₆₈O₁₃
Molecular Weight:817.027
Hs Code.:

Acetic acid (S)-3-benzyloxymethoxy-4-((4S,6S)-6-{(4S,6R)-6-[(S)-2-benzyloxymethoxy-3-((4R,6R)-6-hydroxymethyl-2,2-dimethyl-[1,3]dioxan-4-yl)-propyl]-2,2-dimethyl-[1,3]dioxan-4-ylmethyl}-2,2-dimethyl-[1,3]dioxan-4-yl)-butyl ester

Synonyms:Acetic acid (S)-3-benzyloxymethoxy-4-((4S,6S)-6-{(4S,6R)-6-[(S)-2-benzyloxymethoxy-3-((4R,6R)-6-hydroxymethyl-2,2-dimethyl-[1,3]dioxan-4-yl)-propyl]-2,2-dimethyl-[1,3]dioxan-4-ylmethyl}-2,2-dimethyl-[1,3]dioxan-4-yl)-butyl ester

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Chemical Property of Acetic acid (S)-3-benzyloxymethoxy-4-((4S,6S)-6-{(4S,6R)-6-[(S)-2-benzyloxymethoxy-3-((4R,6R)-6-hydroxymethyl-2,2-dimethyl-[1,3]dioxan-4-yl)-propyl]-2,2-dimethyl-[1,3]dioxan-4-ylmethyl}-2,2-dimethyl-[1,3]dioxan-4-yl)-butyl ester

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Technology Process of Acetic acid (S)-3-benzyloxymethoxy-4-((4S,6S)-6-{(4S,6R)-6-[(S)-2-benzyloxymethoxy-3-((4R,6R)-6-hydroxymethyl-2,2-dimethyl-[1,3]dioxan-4-yl)-propyl]-2,2-dimethyl-[1,3]dioxan-4-ylmethyl}-2,2-dimethyl-[1,3]dioxan-4-yl)-butyl ester

There total 5 articles about Acetic acid (S)-3-benzyloxymethoxy-4-((4S,6S)-6-{(4S,6R)-6-[(S)-2-benzyloxymethoxy-3-((4R,6R)-6-hydroxymethyl-2,2-dimethyl-[1,3]dioxan-4-yl)-propyl]-2,2-dimethyl-[1,3]dioxan-4-ylmethyl}-2,2-dimethyl-[1,3]dioxan-4-yl)-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 883554-56-1
Acetic acid (S)-3-benzyloxymethoxy-4-{(4S,6S)-6-[(4S,6R)-6-((2R,4S,6R)-2-benzyloxymethoxy-4,6,7-trihydroxy-heptyl)-2,2-dimethyl-[1,3]dioxan-4-ylmethyl]-2,2-dimethyl-[1,3]dioxan-4-yl}-butyl ester

: 77-76-9
2,2-dimethoxy-propane

: 883554-57-2
Acetic acid (S)-3-benzyloxymethoxy-4-((4S,6S)-6-{(4S,6R)-6-[(S)-2-benzyloxymethoxy-3-((4R,6R)-6-hydroxymethyl-2,2-dimethyl-[1,3]dioxan-4-yl)-propyl]-2,2-dimethyl-[1,3]dioxan-4-ylmethyl}-2,2-dimethyl-[1,3]dioxan-4-yl)-butyl ester

Guidance literature:: With camphor-10-sulfonic acid; In acetone; at -10 ℃;
DOI:10.1002/ejoc.200500670

Reference yield:

: 883554-54-9
Acetic acid (S)-4-((4S,6S)-6-{(4S,6R)-6-[(R)-4-(tert-butyl-dimethyl-silanyloxy)-2-hydroxy-butyl]-2,2-dimethyl-[1,3]dioxan-4-ylmethyl}-2,2-dimethyl-[1,3]dioxan-4-yl)-3-hydroxy-butyl ester

: 883554-57-2
Acetic acid (S)-3-benzyloxymethoxy-4-((4S,6S)-6-{(4S,6R)-6-[(S)-2-benzyloxymethoxy-3-((4R,6R)-6-hydroxymethyl-2,2-dimethyl-[1,3]dioxan-4-yl)-propyl]-2,2-dimethyl-[1,3]dioxan-4-ylmethyl}-2,2-dimethyl-[1,3]dioxan-4-yl)-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 68 percent / Me₂SO₂NH₂; K₂CO₃; (DHQD)2PHAL / K₂OsO₂(OH)4; K₃Fe(CN)6 / 2-methyl-propan-2-ol; H₂O / 13 h / 0 °C

2: 69 percent / camphorsulfonic acid / acetone / -10 °C

With Me₂SO₂NH₂; camphor-10-sulfonic acid; potassium carbonate; 1,4-bis(9-O-dihydroquinidine)phthalazine; potassium dioxotetrahydroxoosmate(VI); potassium hexacyanoferrate(III); In water; acetone; tert-butyl alcohol;
DOI:10.1002/ejoc.200500670

Reference yield:

: 883554-55-0
Acetic acid (S)-3-benzyloxymethoxy-4-{(4S,6S)-6-[(4S,6R)-6-((2R,4S)-2-benzyloxymethoxy-4-hydroxy-hept-6-enyl)-2,2-dimethyl-[1,3]dioxan-4-ylmethyl]-2,2-dimethyl-[1,3]dioxan-4-yl}-butyl ester

: 883554-57-2
Acetic acid (S)-3-benzyloxymethoxy-4-((4S,6S)-6-{(4S,6R)-6-[(S)-2-benzyloxymethoxy-3-((4R,6R)-6-hydroxymethyl-2,2-dimethyl-[1,3]dioxan-4-yl)-propyl]-2,2-dimethyl-[1,3]dioxan-4-ylmethyl}-2,2-dimethyl-[1,3]dioxan-4-yl)-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / Me₂SO₂NH₂; K₂CO₃; (DHQD)2PHAL / K₂OsO₂(OH)4; K₃Fe(CN)6 / 2-methyl-propan-2-ol; H₂O / 13 h / 0 °C

2: 69 percent / camphorsulfonic acid / acetone / -10 °C

With Me₂SO₂NH₂; camphor-10-sulfonic acid; potassium carbonate; 1,4-bis(9-O-dihydroquinidine)phthalazine; potassium dioxotetrahydroxoosmate(VI); potassium hexacyanoferrate(III); In water; acetone; tert-butyl alcohol;
DOI:10.1002/ejoc.200500670