methyl 4-(but-3-yn-1-yl)-3-hydroxy-2-methoxy-6-(2-methoxy-2-oxoethyl)benzoate

Base Information

Chemical Name:methyl 4-(but-3-yn-1-yl)-3-hydroxy-2-methoxy-6-(2-methoxy-2-oxoethyl)benzoate
CAS No.:1431956-34-1
Molecular Formula:C₁₆H₁₈O₆
Molecular Weight:306.315
Hs Code.:

Synonyms:methyl 4-(but-3-yn-1-yl)-3-hydroxy-2-methoxy-6-(2-methoxy-2-oxoethyl)benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 4-(but-3-yn-1-yl)-3-hydroxy-2-methoxy-6-(2-methoxy-2-oxoethyl)benzoate

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Technology Process of methyl 4-(but-3-yn-1-yl)-3-hydroxy-2-methoxy-6-(2-methoxy-2-oxoethyl)benzoate

There total 4 articles about methyl 4-(but-3-yn-1-yl)-3-hydroxy-2-methoxy-6-(2-methoxy-2-oxoethyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1431956-31-8
C₁₉H₂₄O₇

: 1431956-34-1
methyl 4-(but-3-yn-1-yl)-3-hydroxy-2-methoxy-6-(2-methoxy-2-oxoethyl)benzoate

Guidance literature:: With silica gel supported sodium hydrogen sulfate; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1021/ol400864f

Reference yield:

: 1431956-29-4
methyl 3-(ethoxymethoxy)-2-methoxy-6-(2-methoxy-2-oxoethyl)-4-(3-oxopropyl)benzoate

: 1431956-34-1
methyl 4-(but-3-yn-1-yl)-3-hydroxy-2-methoxy-6-(2-methoxy-2-oxoethyl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / methanol / 20 °C

2: silica gel supported sodium hydrogen sulfate / dichloromethane / 4 h / 20 °C

With silica gel supported sodium hydrogen sulfate; potassium carbonate; In methanol; dichloromethane; 1: |Seyferth-Gilbert Homologation;
DOI:10.1021/ol400864f

Reference yield:

: 1431956-27-2
C₁₈H₂₆O₈

: 1431956-34-1
methyl 4-(but-3-yn-1-yl)-3-hydroxy-2-methoxy-6-(2-methoxy-2-oxoethyl)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridinium chlorochromate; sodium acetate / dichloromethane / 3 h / 20 °C

2: potassium carbonate / methanol / 20 °C

3: silica gel supported sodium hydrogen sulfate / dichloromethane / 4 h / 20 °C

With silica gel supported sodium hydrogen sulfate; sodium acetate; potassium carbonate; pyridinium chlorochromate; In methanol; dichloromethane; 2: |Seyferth-Gilbert Homologation;
DOI:10.1021/ol400864f