methyl 3-(ethoxymethoxy)-2-methoxy-6-(2-methoxy-2-oxoethyl)-4-(3-oxopropyl)benzoate

Base Information

• Chemical Name: methyl 3-(ethoxymethoxy)-2-methoxy-6-(2-methoxy-2-oxoethyl)-4-(3-oxopropyl)benzoate
• CAS No.: 1431956-29-4
• Molecular Formula: C₁₈H₂₄O₈
• Molecular Weight: 368.384

Synonyms:methyl 3-(ethoxymethoxy)-2-methoxy-6-(2-methoxy-2-oxoethyl)-4-(3-oxopropyl)benzoate

Chemical Property of methyl 3-(ethoxymethoxy)-2-methoxy-6-(2-methoxy-2-oxoethyl)-4-(3-oxopropyl)benzoate

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Technology Process of methyl 3-(ethoxymethoxy)-2-methoxy-6-(2-methoxy-2-oxoethyl)-4-(3-oxopropyl)benzoate

There total 2 articles about methyl 3-(ethoxymethoxy)-2-methoxy-6-(2-methoxy-2-oxoethyl)-4-(3-oxopropyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

C18H26O8 (1431956-27-2) → methyl 3-(ethoxymethoxy)-2-methoxy-6-(2-methoxy-2-oxoethyl)-4-(3-oxopropyl)benzoate (1431956-29-4)

Guidance literature:

With sodium acetate; pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 3h;

DOI:10.1021/ol400864f

Reference yield:

methyl 4-allyl-3-(ethoxymethoxy)-2-methoxy-6-(2-methoxy-2-oxoethyl)benzoate (1402733-49-6) → methyl 3-(ethoxymethoxy)-2-methoxy-6-(2-methoxy-2-oxoethyl)-4-(3-oxopropyl)benzoate (1431956-29-4)

Guidance literature:

Multi-step reaction with 2 steps

1: dimethylsulfide borane complex / tetrahydrofuran / 4 h / 0 - 20 °C

2: pyridinium chlorochromate; sodium acetate / dichloromethane / 3 h / 20 °C

With dimethylsulfide borane complex; sodium acetate; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane;

DOI:10.1021/ol400864f

Reference yield: 98.0%

methyl 3-(ethoxymethoxy)-2-methoxy-6-(2-methoxy-2-oxoethyl)-4-(3-oxopropyl)benzoate (1431956-29-4) + dimethyl 1-(1-diazo-2-oxopropyl)phosphonate (90965-06-3) → C19H24O7 (1431956-31-8)

Guidance literature:

With potassium carbonate; In methanol; at 20 ℃;

DOI:10.1021/ol400864f

upstream raw materials:

C₁₈H₂₆O₈

methyl 4-allyl-3-(ethoxymethoxy)-2-methoxy-6-(2-methoxy-2-oxoethyl)benzoate

Downstream raw materials:

methyl-3-(ethoxymethoxy)-4-(4-(3-(ethoxymethoxy)-1,6-dimethoxy-5,8-dioxo-5,8-dihydronaphthalen-2-yl)but-3-yn-1-yl)-2-methoxy-6-(2-methoxy-2-oxoethyl)benzoate

methyl 3-hydroxy-4-(4-(3-hydroxy-1,6-dimethoxy-5,8-dioxo-5,8-dihydronaphthalen-2-yl)but-3-yn-1-yl)-2-methoxy-6-(2-methoxy-2-oxoethyl)benzoate

methyl 4-(4-(3-(ethoxymethoxy)-1,6-dimethoxy-5,8-dioxo-5,8-dihydronaphthalen-2-yl)but-3-yn-1-yl)-3-hydroxy-2-methoxy-6-(2-methoxy-2-oxoethyl)benzoate

methyl 4-(but-3-yn-1-yl)-3-hydroxy-2-methoxy-6-(2-methoxy-2-oxoethyl)benzoate

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