C₂₂H₂₆O₈

Base Information

Chemical Name:C₂₂H₂₆O₈
CAS No.:1375645-35-4
Molecular Formula:C₂₂H₂₆O₈
Molecular Weight:418.444
Hs Code.:

C<sub>22</sub>H<sub>26</sub>O<sub>8</sub>

Synonyms:C₂₂H₂₆O₈

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Chemical Property of C₂₂H₂₆O₈

Chemical Property:

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Technology Process of C₂₂H₂₆O₈

There total 7 articles about C₂₂H₂₆O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1375645-00-3
C₂₂H₂₆O₆

: 1375645-35-4
C₂₂H₂₆O₈

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; In water; isopropyl alcohol; at 0 - 20 ℃; for 8h;
DOI:10.1016/j.tetlet.2012.03.098

Reference yield:

: 1375645-24-1
3-bromomethyl-4-iodofuran

: 1375645-35-4
C₂₂H₂₆O₈

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 2 h / 0 - 20 °C

1.2: 2 h / 70 °C

2.1: dmap; water; sodium chloride / dimethyl sulfoxide / 19 h / 180 °C

3.1: bis-triphenylphosphine-palladium(II) chloride; tri-n-butyl-tin hydride / dichloromethane / 0.5 h / 20 °C

3.2: 1 h / 80 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

5.1: sodium hydroxide / tetrahydrofuran; methanol; water / 1 h / 20 °C

5.2: 20 °C

6.1: dmap; 2-methyl-6-nitrobenzoic anhydride / dichloromethane / 0.5 h / 0 °C

7.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; isopropyl alcohol / 8 h / 0 - 20 °C

With dmap; bis-triphenylphosphine-palladium(II) chloride; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; 2-methyl-6-nitrobenzoic anhydride; tetrabutyl ammonium fluoride; water; tri-n-butyl-tin hydride; sodium hydride; sodium chloride; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; isopropyl alcohol; 2.1: Krapcho decarboalkoxylation / 3.2: Stille coupling;
DOI:10.1016/j.tetlet.2012.03.098

Reference yield:

: 1375645-31-0
C₂₄H₃₂O₇

: 1375645-35-4
C₂₂H₂₆O₈

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide / tetrahydrofuran; methanol; water / 1 h / 20 °C

1.2: 20 °C

2.1: dmap; 2-methyl-6-nitrobenzoic anhydride / dichloromethane / 0.5 h / 0 °C

3.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; isopropyl alcohol / 8 h / 0 - 20 °C

With dmap; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; 2-methyl-6-nitrobenzoic anhydride; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; isopropyl alcohol;
DOI:10.1016/j.tetlet.2012.03.098