3-decynoyl chloride

Base Information

• Chemical Name: 3-decynoyl chloride
• CAS No.: 124576-41-6
• Molecular Formula: C₁₀H₁₅ClO
• Molecular Weight: 186.681
• Mol file: 124576-41-6.mol

Synonyms:3-decynoyl chloride

Chemical Property of 3-decynoyl chloride

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 3-decynoyl chloride

There total 1 articles about 3-decynoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-butynoic acid (2345-51-9) + 1-Iodohexane (638-45-9) → dec-3-ynoic acid (27007-78-9) + 3-decynoyl chloride (124576-41-6)

Guidance literature:

With n-butyllithium; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane;

Reference yield: 13.0%

(4R)-N-(3-((2-hydroxyethyl)amino)-3-oxopropyl)-2-(4-methoxyphenyl)-5,5-dimethyl-1,3-dioxane-4-carboxamide + 3-decynoyl chloride (124576-41-6) → C29H42N2O7

Guidance literature:

With pyridine; In dichloromethane; at 0 ℃; Inert atmosphere;

DOI:10.1016/j.bmcl.2010.06.028

Reference yield:

3-decynoyl chloride (124576-41-6) → (3E)-dec-3-enoic acid (2430-93-5,15469-77-9,53678-20-9)

Guidance literature:

nickel boride; In hydrogenchloride; methanol;

upstream raw materials:

3-butynoic acid

1-Iodohexane

Downstream raw materials:

(3E)-dec-3-enoic acid