N-{4-[(2-dimethylamino-ethylimino)-methyl]-benzylidene}-N',N'-dimethyl-ethane-1,2-diamine

Base Information

• Chemical Name: N-{4-[(2-dimethylamino-ethylimino)-methyl]-benzylidene}-N',N'-dimethyl-ethane-1,2-diamine
• CAS No.: 214679-95-5
• Molecular Formula: C₁₆H₂₆N₄
• Molecular Weight: 274.409

Synonyms:N-{4-[(2-dimethylamino-ethylimino)-methyl]-benzylidene}-N',N'-dimethyl-ethane-1,2-diamine

Chemical Property of N-{4-[(2-dimethylamino-ethylimino)-methyl]-benzylidene}-N',N'-dimethyl-ethane-1,2-diamine

Chemical Property:

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Technology Process of N-{4-[(2-dimethylamino-ethylimino)-methyl]-benzylidene}-N',N'-dimethyl-ethane-1,2-diamine

There total 1 articles about N-{4-[(2-dimethylamino-ethylimino)-methyl]-benzylidene}-N',N'-dimethyl-ethane-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

terephthalaldehyde, (623-27-8) + N,N-dimethylethylenediamine (108-00-9) → N-{4-[(2-dimethylamino-ethylimino)-methyl]-benzylidene}-N',N'-dimethyl-ethane-1,2-diamine (214679-95-5)

Guidance literature:

In toluene; for 0.5h; Yield given;

Reference yield: 88.0%

bis[dimethyl(μ-dimethylsulfide)platinum(II)] + N-{4-[(2-dimethylamino-ethylimino)-methyl]-benzylidene}-N',N'-dimethyl-ethane-1,2-diamine (214679-95-5) → (CH3)2Pt(CH3)2NCH2CH2NCHC6H4CHNCH2CH2N(CH3)2Pt(CH3)2 (680575-95-5,235432-93-6)

Guidance literature:

In diethyl ether; (N2); addn. of a soln. of ligand in Et2O to a soln. of platinum complex in Et2O, keeping for 40 min; concn., addn. of pentane, filtration, washing with ether, pentane, drying in vac.; elem. anal.;

DOI:10.1021/om030650m

Reference yield:

N-{4-[(2-dimethylamino-ethylimino)-methyl]-benzylidene}-N',N'-dimethyl-ethane-1,2-diamine (214679-95-5) → CH3PtCl(CH3)2NCH2CH2NCHC6H4CHNCH2CH2N(CH3)2Pt(CH3)2 (680576-05-0)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether

2: dichloromethane-d2

In diethyl ether; dichloromethane-d2;

DOI:10.1021/om030650m

upstream raw materials:

terephthalaldehyde,

N,N-dimethylethylenediamine

Downstream raw materials:

(CH₃)2Pt(CH₃)2NCH₂CH₂NCHC₆H₄CHNCH₂CH₂N(CH₃)2Pt(CH₃)2

CH₃PtCl(CH₃)2NCH₂CH₂NCHC₆H₄CHNCH₂CH₂N(CH₃)2Pt(CH₃)2

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