(3aS,5R,6R,7R)-5-Benzenesulfonyl-6-methoxy-7-methoxymethoxy-5-methyl-3,3a,4,5,6,7-hexahydro-benzo[c]isoxazole

Base Information

• Chemical Name: (3aS,5R,6R,7R)-5-Benzenesulfonyl-6-methoxy-7-methoxymethoxy-5-methyl-3,3a,4,5,6,7-hexahydro-benzo[c]isoxazole
• CAS No.: 103246-51-1
• Molecular Formula: C₁₇H₂₃NO₆S
• Molecular Weight: 369.439

Synonyms:(3aS,5R,6R,7R)-5-Benzenesulfonyl-6-methoxy-7-methoxymethoxy-5-methyl-3,3a,4,5,6,7-hexahydro-benzo[c]isoxazole

Chemical Property of (3aS,5R,6R,7R)-5-Benzenesulfonyl-6-methoxy-7-methoxymethoxy-5-methyl-3,3a,4,5,6,7-hexahydro-benzo[c]isoxazole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (3aS,5R,6R,7R)-5-Benzenesulfonyl-6-methoxy-7-methoxymethoxy-5-methyl-3,3a,4,5,6,7-hexahydro-benzo[c]isoxazole

There total 30 articles about (3aS,5R,6R,7R)-5-Benzenesulfonyl-6-methoxy-7-methoxymethoxy-5-methyl-3,3a,4,5,6,7-hexahydro-benzo[c]isoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

(R)-4-Benzenesulfonyl-3-methoxy-2-methoxymethoxy-4-methyl-hept-6-enal oxime (103246-50-0,103257-96-1) → (3aS,5R,6R,7R)-5-Benzenesulfonyl-6-methoxy-7-methoxymethoxy-5-methyl-3,3a,4,5,6,7-hexahydro-benzo[c]isoxazole (103246-51-1) + (3aS,5R,6S,7R)-5-Benzenesulfonyl-6-methoxy-7-methoxymethoxy-5-methyl-3,3a,4,5,6,7-hexahydro-benzo[c]isoxazole (103246-51-1,103303-56-6) + (3aR,5S,6R,7R)-5-Benzenesulfonyl-6-methoxy-7-methoxymethoxy-5-methyl-3,3a,4,5,6,7-hexahydro-benzo[c]isoxazole (103303-56-6) + (3aR,5S,6S,7R)-5-Benzenesulfonyl-6-methoxy-7-methoxymethoxy-5-methyl-3,3a,4,5,6,7-hexahydro-benzo[c]isoxazole (103246-51-1,103303-56-6)

Guidance literature:

With sodium hypochlorite; In triethylamine;

DOI:10.1016/S0040-4039(00)98918-4

Reference yield: 48.0%

(R)-4-Benzenesulfonyl-3-methoxy-2-methoxymethoxy-4-methyl-hept-6-enal oxime (103246-50-0,103257-96-1) → (3aS,5R,6R,7R)-5-Benzenesulfonyl-6-methoxy-7-methoxymethoxy-5-methyl-3,3a,4,5,6,7-hexahydro-benzo[c]isoxazole (103246-51-1) + (3aS,5R,6S,7R)-5-Benzenesulfonyl-6-methoxy-7-methoxymethoxy-5-methyl-3,3a,4,5,6,7-hexahydro-benzo[c]isoxazole (103246-51-1,103303-56-6) + (3aR,5S,6R,7R)-5-Benzenesulfonyl-6-methoxy-7-methoxymethoxy-5-methyl-3,3a,4,5,6,7-hexahydro-benzo[c]isoxazole (103303-56-6) + (3aR,5S,6S,7R)-5-Benzenesulfonyl-6-methoxy-7-methoxymethoxy-5-methyl-3,3a,4,5,6,7-hexahydro-benzo[c]isoxazole (103246-51-1,103303-56-6)

Guidance literature:

With sodium hypochlorite; In triethylamine;

DOI:10.1016/S0040-4039(00)98918-4

Reference yield: 48.0%

(R)-4-Benzenesulfonyl-3-methoxy-2-methoxymethoxy-4-methyl-hept-6-enal oxime (103246-50-0,103257-96-1) → (3aS,5R,6R,7R)-5-Benzenesulfonyl-6-methoxy-7-methoxymethoxy-5-methyl-3,3a,4,5,6,7-hexahydro-benzo[c]isoxazole (103246-51-1) + (3aS,5R,6S,7R)-5-Benzenesulfonyl-6-methoxy-7-methoxymethoxy-5-methyl-3,3a,4,5,6,7-hexahydro-benzo[c]isoxazole (103246-51-1,103303-56-6) + (3aR,5S,6R,7R)-5-Benzenesulfonyl-6-methoxy-7-methoxymethoxy-5-methyl-3,3a,4,5,6,7-hexahydro-benzo[c]isoxazole (103303-56-6) + (3aR,5S,6S,7R)-5-Benzenesulfonyl-6-methoxy-7-methoxymethoxy-5-methyl-3,3a,4,5,6,7-hexahydro-benzo[c]isoxazole (103246-51-1,103303-56-6)

Guidance literature:

With sodium hypochlorite; In triethylamine;

DOI:10.1016/S0040-4039(00)98918-4

upstream raw materials:

(R)-4-Benzenesulfonyl-3-methoxy-2-methoxymethoxy-4-methyl-hept-6-enal oxime

ethyl phenyl sulfone

2,2-Dimethyl-propionic acid (R)-4-benzenesulfonyl-3-methoxy-2-methoxymethoxy-4-methyl-hept-6-enyl ester

4-(phenylsulfonyl)pent-1-en

Downstream raw materials:

(2S,3R,4R,6R)-4-Benzenesulfonyl-2-(2-bromo-allyloxy)-6-(tert-butyl-dimethyl-silanyloxymethyl)-3-methoxy-4-methyl-cyclohexanone

(3aS,5R,6R,7R)-5-Benzenesulfonyl-7-(2-bromo-allyloxy)-6-methoxy-5-methyl-3,3a,4,5,6,7-hexahydro-benzo[c]isoxazole

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