1'-(4-biphenylmethyl)-1-bromoferrocene

Base Information

Chemical Name:1'-(4-biphenylmethyl)-1-bromoferrocene
CAS No.:263261-14-9
Molecular Formula:C₂₃H₁₉BrFe
Molecular Weight:431.155
Hs Code.:

Synonyms:1'-(4-biphenylmethyl)-1-bromoferrocene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1'-(4-biphenylmethyl)-1-bromoferrocene

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Technology Process of 1'-(4-biphenylmethyl)-1-bromoferrocene

There total 1 articles about 1'-(4-biphenylmethyl)-1-bromoferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 263261-10-5
1'-(4-biphenylcarbonyl)-1-bromoferrocene

: 263261-14-9
1'-(4-biphenylmethyl)-1-bromoferrocene

Guidance literature:: With LiAlH₄; AlCl₃; In diethyl ether; under N2, AlCl3 was added to ethereal soln. of Fe-complex and LiAlH4, stirring for 1 h; H2O was added, ethereal layer was sepd., washed with H2O, dried over MgSO4, solvent was evapd., chromy. (neutral alumina, hexane);
DOI:10.1021/om9908884

Reference yield: 75.0%

: 263261-14-9
1'-(4-biphenylmethyl)-1-bromoferrocene

: 263261-08-1
1',1'''-bis(4-diphenylmethyl)biferrocene

Guidance literature:: With activated Cu; In neat (no solvent); under N2, Fe-complex and activated Cu (1:5 mass ratio) were heated underN2 at 120-130 °C for 24 h; mixt. was cooled to room temp., extd. with CH2Cl2 until extract appearedcolorless, extract was evapd. and chromd. (neutral alumina) elution wit h hexane (starting material) then with CH2Cl2, recrystn. from hexane/benzene;
DOI:10.1021/om9908884