(E)-3-[4-(2-aminoethylamino)-3-nitrophenyl]acrylic acid methyl ester hydrochloride

Base Information

Chemical Name:(E)-3-[4-(2-aminoethylamino)-3-nitrophenyl]acrylic acid methyl ester hydrochloride
CAS No.:1312574-49-4
Molecular Formula:C₁₂H₁₅N₃O₄*ClH
Molecular Weight:301.73
Hs Code.:

Synonyms:(E)-3-[4-(2-aminoethylamino)-3-nitrophenyl]acrylic acid methyl ester hydrochloride

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Chemical Property of (E)-3-[4-(2-aminoethylamino)-3-nitrophenyl]acrylic acid methyl ester hydrochloride

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Technology Process of (E)-3-[4-(2-aminoethylamino)-3-nitrophenyl]acrylic acid methyl ester hydrochloride

There total 3 articles about (E)-3-[4-(2-aminoethylamino)-3-nitrophenyl]acrylic acid methyl ester hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 929018-81-5
(E)-3-[4-(2-(tert-butoxycarbonylamino)ethylamino)-3-nitrophenyl]acrylic acid methyl ester

: 1312574-49-4
(E)-3-[4-(2-aminoethylamino)-3-nitrophenyl]acrylic acid methyl ester hydrochloride

Guidance literature:: With hydrogenchloride; In methanol; at 65 - 70 ℃; for 3h;
DOI:10.1021/jm2003552

Reference yield:

: 877065-30-0
3-(4-chloro-3-nitrophenyl)acrylic acid methyl ester

: 1312574-49-4
(E)-3-[4-(2-aminoethylamino)-3-nitrophenyl]acrylic acid methyl ester hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / 1,4-dioxane / 80 - 100 °C

2: hydrogenchloride / methanol / 3 h / 65 - 70 °C

With hydrogenchloride; triethylamine; In 1,4-dioxane; methanol;
DOI:10.1021/jm2003552

Reference yield:

: 20797-48-2,199679-38-4
(E)-4-chloro-3-nitrocinnamic acid

: 1312574-49-4
(E)-3-[4-(2-aminoethylamino)-3-nitrophenyl]acrylic acid methyl ester hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid / 80 - 85 °C

2: triethylamine / 1,4-dioxane / 80 - 100 °C

3: hydrogenchloride / methanol / 3 h / 65 - 70 °C

With hydrogenchloride; sulfuric acid; triethylamine; In 1,4-dioxane; methanol;
DOI:10.1021/jm2003552