N-{4-[(1,1-dimethylethoxy)carbonylamino]phenyl}-1,2-dithiolane-3-pentanamide

Base Information

Chemical Name:N-{4-[(1,1-dimethylethoxy)carbonylamino]phenyl}-1,2-dithiolane-3-pentanamide
CAS No.:299189-12-1
Molecular Formula:C₁₉H₂₈N₂O₃S₂
Molecular Weight:396.575
Hs Code.:

Synonyms:N-{4-[(1,1-dimethylethoxy)carbonylamino]phenyl}-1,2-dithiolane-3-pentanamide

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Chemical Property of N-{4-[(1,1-dimethylethoxy)carbonylamino]phenyl}-1,2-dithiolane-3-pentanamide

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Technology Process of N-{4-[(1,1-dimethylethoxy)carbonylamino]phenyl}-1,2-dithiolane-3-pentanamide

There total 2 articles about N-{4-[(1,1-dimethylethoxy)carbonylamino]phenyl}-1,2-dithiolane-3-pentanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.5%

: 71026-66-9
N-(tert-butoxycarbonyl)-1,4-phenylenediamine

: 1077-28-7,62-46-4
Thioctic acid

: 299189-12-1
N-{4-[(1,1-dimethylethoxy)carbonylamino]phenyl}-1,2-dithiolane-3-pentanamide

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 25 ℃;
DOI:10.1016/S0960-894X(02)00216-0

Reference yield: 80.5%

: 1-(3-dimethylaminopropyl-3-ethyl-carbodiimide hydrochloride

: 71026-66-9
N-(tert-butoxycarbonyl)-1,4-phenylenediamine

: 1077-28-7,62-46-4
Thioctic acid

: 299189-12-1
N-{4-[(1,1-dimethylethoxy)carbonylamino]phenyl}-1,2-dithiolane-3-pentanamide

Guidance literature:: With triethylamine; In dichloromethane; water;

Reference yield: 29.0%

: 299189-12-1
N-{4-[(1,1-dimethylethoxy)carbonylamino]phenyl}-1,2-dithiolane-3-pentanamide

: 299189-13-2
N-(4-aminophenyl)-5-(1,2-dithiolane-3-yl)pentanamide

Guidance literature:: With hydrogenchloride; ethanol; In diethyl ether; dichloromethane; acetone; at 0 - 20 ℃;
DOI:10.1016/S0960-894X(02)00216-0