2-Chloro-5-cyclohexylmethyl-3-(3-cyclohexylmethyl-2-hydroxy-4,5-dimethoxy-phenyl)-6-methoxy-[1,4]benzoquinone

Base Information

Chemical Name:2-Chloro-5-cyclohexylmethyl-3-(3-cyclohexylmethyl-2-hydroxy-4,5-dimethoxy-phenyl)-6-methoxy-[1,4]benzoquinone
CAS No.:180912-61-2
Molecular Formula:C₂₉H₃₇ClO₆
Molecular Weight:517.062
Hs Code.:

Synonyms:2-Chloro-5-cyclohexylmethyl-3-(3-cyclohexylmethyl-2-hydroxy-4,5-dimethoxy-phenyl)-6-methoxy-[1,4]benzoquinone

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Chemical Property of 2-Chloro-5-cyclohexylmethyl-3-(3-cyclohexylmethyl-2-hydroxy-4,5-dimethoxy-phenyl)-6-methoxy-[1,4]benzoquinone

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Technology Process of 2-Chloro-5-cyclohexylmethyl-3-(3-cyclohexylmethyl-2-hydroxy-4,5-dimethoxy-phenyl)-6-methoxy-[1,4]benzoquinone

There total 10 articles about 2-Chloro-5-cyclohexylmethyl-3-(3-cyclohexylmethyl-2-hydroxy-4,5-dimethoxy-phenyl)-6-methoxy-[1,4]benzoquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 180912-48-5
2-cyclohexylmethyl-3,4-dimethoxyphenol

: 180912-59-8
2,3-Dichloro-5-cyclohexylmethyl-6-methoxy-[1,4]benzoquinone

: 180912-61-2
2-Chloro-5-cyclohexylmethyl-3-(3-cyclohexylmethyl-2-hydroxy-4,5-dimethoxy-phenyl)-6-methoxy-[1,4]benzoquinone

Guidance literature:: With sodium hydride; In tetrahydrofuran; -78 up to -35 deg C;
DOI:10.1016/0040-4039(96)01209-9

Reference yield:

: 57234-28-3
1-methoxy-3-(methoxymethoxy)benzene

: 180912-61-2
2-Chloro-5-cyclohexylmethyl-3-(3-cyclohexylmethyl-2-hydroxy-4,5-dimethoxy-phenyl)-6-methoxy-[1,4]benzoquinone

Guidance literature:: Multi-step reaction with 6 steps

1: 87 percent / t-BuLi / hexane / 0 °C

2: 91 percent / H₂ / 10percent Pd/C / methanol / Ambient temperature

3: 92 percent / conc. HCl / methanol / Ambient temperature

4: 73 percent / salcomine, O₂ / dimethylformamide / Ambient temperature

5: 62 percent / SOCl₂, pyridine / benzene / Heating

6: 85 percent / NaH / tetrahydrofuran / -78 up to -35 deg C

With pyridine; hydrogenchloride; thionyl chloride; salcomine; hydrogen; tert.-butyl lithium; oxygen; sodium hydride; palladium on activated charcoal; In tetrahydrofuran; methanol; hexane; N,N-dimethyl-formamide; benzene;
DOI:10.1016/0040-4039(96)01209-9

Reference yield:

: 133129-56-3
1,2-dimethoxy-4-(methoxymethoxy)benzene

: 180912-61-2
2-Chloro-5-cyclohexylmethyl-3-(3-cyclohexylmethyl-2-hydroxy-4,5-dimethoxy-phenyl)-6-methoxy-[1,4]benzoquinone

Guidance literature:: Multi-step reaction with 4 steps

1: 41 percent / t-BuLi / hexane / 0 °C

2: 49 percent / H₂ / 10percent Pd/C / methanol / Ambient temperature

3: 86 percent / conc. HCl / methanol / Ambient temperature

4: 85 percent / NaH / tetrahydrofuran / -78 up to -35 deg C

With hydrogenchloride; hydrogen; tert.-butyl lithium; sodium hydride; palladium on activated charcoal; In tetrahydrofuran; methanol; hexane;
DOI:10.1016/0040-4039(96)01209-9