C₅₃H₇₁NO₉Si

Base Information

Chemical Name:C₅₃H₇₁NO₉Si
CAS No.:927662-01-9
Molecular Formula:C₅₃H₇₁NO₉Si
Molecular Weight:894.234
Hs Code.:

C<sub>53</sub>H<sub>71</sub>NO<sub>9</sub>Si

Synonyms:C₅₃H₇₁NO₉Si

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Chemical Property of C₅₃H₇₁NO₉Si

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Technology Process of C₅₃H₇₁NO₉Si

There total 9 articles about C₅₃H₇₁NO₉Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 927661-97-0
C₂₇H₃₈O₅Si

: 927661-99-2
C₂₅H₃₄O₅

: 7677-24-9
trimethylsilyl cyanide

: 927662-01-9
C₅₃H₇₁NO₉Si

Guidance literature:: C₂₇H₃₈O₅Si; C₂₅H₃₄O₅; trimethylsilyl cyanide; With scandium tris(trifluoromethanesulfonate); In dichloromethane; at 20 ℃; for 18h;

With potassium carbonate; In methanol; at 20 ℃; Further stages.;
DOI:10.3987/COM-06-S(O)23

Reference yield:

: 927661-96-9
C₂₇H₃₈O₄Si

: 927662-01-9
C₅₃H₇₁NO₉Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: 9-BBN / tetrahydrofuran / 3 h / 20 °C / sonication

1.2: H₂O₂; aq. NaHCO₃ / tetrahydrofuran / 1 h / 20 °C

1.3: 99 percent / Dess-Martin periodinane / CH₂Cl₂ / 0.58 h / 20 °C

2.1: 78 percent / Sc(OTf)3 / benzene / 14 h / 20 °C

3.1: Sc(OTf)3 / CH₂Cl₂ / 9.5 h / 20 °C

3.2: 92 percent / K₂CO₃ / methanol / 0.5 h / 20 °C

With 9-borabicyclo[3.3.1]nonane dimer; scandium tris(trifluoromethanesulfonate); In tetrahydrofuran; dichloromethane; benzene;
DOI:10.3987/COM-06-S(O)23

Reference yield:

: 927661-98-1
C₃₁H₄₅NO₄Si

: 927662-01-9
C₅₃H₇₁NO₉Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: DIBAL-H / CH₂Cl₂ / -78 °C

1.2: NaBH₄ / ethanol / 1.5 h / 20 °C

1.3: 78 percent / TBAF / tetrahydrofuran / 1 h / 20 °C

2.1: 78 percent / Sc(OTf)3 / benzene / 14 h / 20 °C

3.1: Sc(OTf)3 / CH₂Cl₂ / 9.5 h / 20 °C

3.2: 92 percent / K₂CO₃ / methanol / 0.5 h / 20 °C

With diisobutylaluminium hydride; scandium tris(trifluoromethanesulfonate); In dichloromethane; benzene;
DOI:10.3987/COM-06-S(O)23