exo-5-benzoylbicyclo<2.1.0>pentane

Base Information

Chemical Name:exo-5-benzoylbicyclo<2.1.0>pentane
CAS No.:94324-07-9
Molecular Formula:C₁₂H₁₂O
Molecular Weight:172.227
Hs Code.:

Synonyms:exo-5-benzoylbicyclo<2.1.0>pentane

Suppliers and Price of exo-5-benzoylbicyclo<2.1.0>pentane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of exo-5-benzoylbicyclo<2.1.0>pentane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of exo-5-benzoylbicyclo<2.1.0>pentane

There total 8 articles about exo-5-benzoylbicyclo<2.1.0>pentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 582298-99-5
1-cyclobutyl-2-oxo-2-phenylethyl 4-methylbenzene-1-sulfonate

: 582299-31-8
(E)-3-cyclopropyl-1-phenylprop-2-en-1-one

: 94324-07-9
exo-5-benzoylbicyclo<2.1.0>pentane

Guidance literature:: With 1-methyl-1H-imidazole; In dichloromethane; UV-irradiation;
DOI:10.1002/hlca.200390086

Reference yield: 58.0%

: 591-51-5
phenyllithium

: 71049-72-4
exo-bicyclo<2.1.0>pentane-5-carboxylic acid

: 94324-07-9
exo-5-benzoylbicyclo<2.1.0>pentane

Guidance literature:: In diethyl ether; for 0.333333h; Ambient temperature;
DOI:10.1021/ja00290a041

Reference yield:

: 4415-82-1
cyclobutanemethanol

: 94324-07-9
exo-5-benzoylbicyclo<2.1.0>pentane

Guidance literature:: Multi-step reaction with 5 steps

1: pyridinium chlorochromate / CH₂Cl₂

2: (i-Pr)2NH; BuLi / diethyl ether; hexane / -78 - -70 °C

3: aq. HF / acetonitrile / 0 °C

4: 74 percent / pyridine / CH₂Cl₂ / 0 °C

5: 61 percent / 1-methyl-1H-imidazole / CH₂Cl₂ / UV-irradiation

With pyridine; 1-methyl-1H-imidazole; n-butyllithium; hydrogen fluoride; diisopropylamine; pyridinium chlorochromate; In diethyl ether; hexane; dichloromethane; acetonitrile;
DOI:10.1002/hlca.200390086