ethyl 4-[4-(acetylamino)-3-({[3-chloro-5-(trifluoromethyl)-2-pyridinyl]methyl}amino)phenoxy]-2,2-dimethylbutanoate

Base Information

Chemical Name:ethyl 4-[4-(acetylamino)-3-({[3-chloro-5-(trifluoromethyl)-2-pyridinyl]methyl}amino)phenoxy]-2,2-dimethylbutanoate
CAS No.:808747-19-5
Molecular Formula:C₂₃H₂₇ClF₃N₃O₄
Molecular Weight:501.933
Hs Code.:

Synonyms:ethyl 4-[4-(acetylamino)-3-({[3-chloro-5-(trifluoromethyl)-2-pyridinyl]methyl}amino)phenoxy]-2,2-dimethylbutanoate

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Chemical Property of ethyl 4-[4-(acetylamino)-3-({[3-chloro-5-(trifluoromethyl)-2-pyridinyl]methyl}amino)phenoxy]-2,2-dimethylbutanoate

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Technology Process of ethyl 4-[4-(acetylamino)-3-({[3-chloro-5-(trifluoromethyl)-2-pyridinyl]methyl}amino)phenoxy]-2,2-dimethylbutanoate

There total 4 articles about ethyl 4-[4-(acetylamino)-3-({[3-chloro-5-(trifluoromethyl)-2-pyridinyl]methyl}amino)phenoxy]-2,2-dimethylbutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: [3-chloro-5-(trifluoromethyl)-2-pyridinyl]methyl methanesulfonate

: 808747-09-3
ethyl 4-[4-(acetylamino)-3-aminophenoxy]-2,2-dimethylbutanoate

: 808747-19-5
ethyl 4-[4-(acetylamino)-3-({[3-chloro-5-(trifluoromethyl)-2-pyridinyl]methyl}amino)phenoxy]-2,2-dimethylbutanoate

Guidance literature:: With potassium carbonate; sodium iodide; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 3h;

Reference yield:

: 808747-08-2
ethyl 4-[4-(acetylamino)-3-nitrophenoxy]-2,2-dimethylbutanoate

: 808747-19-5
ethyl 4-[4-(acetylamino)-3-({[3-chloro-5-(trifluoromethyl)-2-pyridinyl]methyl}amino)phenoxy]-2,2-dimethylbutanoate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium 10% on activated carbon / tetrahydrofuran; ethanol / 6 h / 20 °C / 760.05 Torr

2: potassium carbonate; sodium iodide / DMF (N,N-dimethyl-formamide) / 3 h / 20 °C

With hydrogen; potassium carbonate; sodium iodide; palladium 10% on activated carbon; In tetrahydrofuran; DMF (N,N-dimethyl-formamide); ethanol;

Reference yield:

: 61404-40-8
ethyl α,α-dimethyl-γ-bromobutyrate

: 808747-19-5
ethyl 4-[4-(acetylamino)-3-({[3-chloro-5-(trifluoromethyl)-2-pyridinyl]methyl}amino)phenoxy]-2,2-dimethylbutanoate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / DMF (N,N-dimethyl-formamide) / 5 h / 20 - 80 °C

2: hydrogen / palladium 10% on activated carbon / tetrahydrofuran; ethanol / 6 h / 20 °C / 760.05 Torr

3: potassium carbonate; sodium iodide / DMF (N,N-dimethyl-formamide) / 3 h / 20 °C

With hydrogen; potassium carbonate; sodium iodide; palladium 10% on activated carbon; In tetrahydrofuran; DMF (N,N-dimethyl-formamide); ethanol;