Technology Process of C49H56O8SSi
There total 18 articles about C49H56O8SSi which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1H-imidazole;
In
N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 84 percent / Ph3P, DEAD / tetrahydrofuran / Heating
2: 98 percent / DIBAL-H / toluene / -78 °C
3: acetonitrile
4: NaOH / H2O / Heating
5: 1.) LDA, 2.) t-BuOK / 1.) THF, -78 deg C, 2.) THF, -78 deg C to r.t.
6: H2O, TFA / CH2Cl2
7: 87 percent / imidazole / dimethylformamide
With
1H-imidazole; sodium hydroxide; potassium tert-butylate; water; diisobutylaluminium hydride; triphenylphosphine; trifluoroacetic acid; lithium diisopropyl amide; diethylazodicarboxylate;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 10 steps
1: 87 percent / BF3*Et2O / CH2Cl2
2: 100 percent / K2CO3, MeOH
3: 68 percent / CSA / methanol / Heating
4: 95 percent / NaH / dimethylformamide
5: Et3N / CH2Cl2 / -78 °C
6: dimethylformamide; acetonitrile
7: 90 percent / DIBAL-H / toluene / -78 °C
8: 1.) LDA, 2.) t-BuOK / 1.) THF, -78 deg C, 2.) THF, -78 deg C to r.t.
9: H2O, TFA / CH2Cl2
10: 87 percent / imidazole / dimethylformamide
With
1H-imidazole; methanol; camphor-10-sulfonic acid; boron trifluoride diethyl etherate; potassium tert-butylate; water; sodium hydride; diisobutylaluminium hydride; potassium carbonate; triethylamine; trifluoroacetic acid; lithium diisopropyl amide;
In
methanol; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;
