(2S,3S)-5-Benzyloxy-2-ethyl-3-phenylsulfanyl-pentanoic acid methoxy-amide

Base Information

Chemical Name:(2S,3S)-5-Benzyloxy-2-ethyl-3-phenylsulfanyl-pentanoic acid methoxy-amide
CAS No.:153499-89-9
Molecular Formula:C₂₁H₂₇NO₃S
Molecular Weight:373.516
Hs Code.:

Synonyms:(2S,3S)-5-Benzyloxy-2-ethyl-3-phenylsulfanyl-pentanoic acid methoxy-amide

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Chemical Property of (2S,3S)-5-Benzyloxy-2-ethyl-3-phenylsulfanyl-pentanoic acid methoxy-amide

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Technology Process of (2S,3S)-5-Benzyloxy-2-ethyl-3-phenylsulfanyl-pentanoic acid methoxy-amide

There total 8 articles about (2S,3S)-5-Benzyloxy-2-ethyl-3-phenylsulfanyl-pentanoic acid methoxy-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 593-56-6
N-methoxylamine hydrochloride

: 153499-88-8
(2S,3S)-5-Benzyloxy-2-ethyl-3-phenylsulfanyl-pentanoic acid

: 153499-89-9
(2S,3S)-5-Benzyloxy-2-ethyl-3-phenylsulfanyl-pentanoic acid methoxy-amide

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;

Reference yield: 84.0%

: 593-56-6
N-methoxylamine hydrochloride

: 153499-85-5
(S)-3-((2S,3S)-5-Benzyloxy-2-ethyl-3-phenylsulfanyl-pentanoyl)-4-isopropyl-oxazolidin-2-one

: 153499-89-9
(2S,3S)-5-Benzyloxy-2-ethyl-3-phenylsulfanyl-pentanoic acid methoxy-amide

: (1'S,2S,3S)-2-ethyl-N-[2'-(methoxyaminocarbonyloxy)-1'-(1-methylethyl)ethyl]-5-benzyloxy-3-(phenylsulfanyl)pentanamide

Guidance literature:: With trimethylaluminum; In tetrahydrofuran; hexane; at 0 ℃; for 7h;
DOI:10.1039/a802419g

Reference yield:

: 153499-90-2
(S)-3-((E)-5-Benzyloxy-2-ethyl-pent-2-enoyl)-4-isopropyl-oxazolidin-2-one

: 153499-89-9
(2S,3S)-5-Benzyloxy-2-ethyl-3-phenylsulfanyl-pentanoic acid methoxy-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / n-BuLi / tetrahydrofuran; hexane / 5 h / -78 °C

2: 5 percent / AlMe₃ / tetrahydrofuran; hexane / 7 h / 0 °C

With n-butyllithium; trimethylaluminum; In tetrahydrofuran; hexane;
DOI:10.1039/a802419g