N'-Benzoyl-N-(4-chloro-benzyl)-N'-methyl-hydrazinecarboxylic acid benzyl ester

Base Information

Chemical Name:N'-Benzoyl-N-(4-chloro-benzyl)-N'-methyl-hydrazinecarboxylic acid benzyl ester
CAS No.:1027411-30-8
Molecular Formula:C₂₃H₂₁ClN₂O₃
Molecular Weight:408.884
Hs Code.:

Synonyms:N'-Benzoyl-N-(4-chloro-benzyl)-N'-methyl-hydrazinecarboxylic acid benzyl ester

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Chemical Property of N'-Benzoyl-N-(4-chloro-benzyl)-N'-methyl-hydrazinecarboxylic acid benzyl ester

Chemical Property:

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Technology Process of N'-Benzoyl-N-(4-chloro-benzyl)-N'-methyl-hydrazinecarboxylic acid benzyl ester

There total 7 articles about N'-Benzoyl-N-(4-chloro-benzyl)-N'-methyl-hydrazinecarboxylic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 98-88-4
benzoyl chloride

: 194664-43-2
N-(4-Chloro-benzyl)-N'-methyl-hydrazinecarboxylic acid benzyl ester

: 1027411-30-8
N'-Benzoyl-N-(4-chloro-benzyl)-N'-methyl-hydrazinecarboxylic acid benzyl ester

Guidance literature:: With pyridine;
DOI:10.1039/a703008h

Reference yield:

: 5331-43-1
N-benzyloxycarbonyl-hydrazine

: 1027411-30-8
N'-Benzoyl-N-(4-chloro-benzyl)-N'-methyl-hydrazinecarboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: 94 percent / pyridine

2: 93 percent / DMAP / acetonitrile

3: 99 percent / PPh₃, DEAD / tetrahydrofuran

4: 99 percent / Al(Hg), CO₂, H₂O / diethyl ether

5: 99 percent / K₂CO₃, NaOH, Bu₄NHSO₄ / benzene

6: 99 percent / TFA / CH₂Cl₂

7: 99 percent / pyridine

With pyridine; dmap; sodium hydroxide; aluminum amalgam; carbon dioxide; water; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; triphenylphosphine; trifluoroacetic acid; diethylazodicarboxylate; In tetrahydrofuran; diethyl ether; dichloromethane; acetonitrile; benzene;
DOI:10.1039/a703008h

Reference yield:

: 194664-23-8
C₁₅H₁₃N₃O₄S

: 1027411-30-8
N'-Benzoyl-N-(4-chloro-benzyl)-N'-methyl-hydrazinecarboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 93 percent / DMAP / acetonitrile

2: 99 percent / PPh₃, DEAD / tetrahydrofuran

3: 99 percent / Al(Hg), CO₂, H₂O / diethyl ether

4: 99 percent / K₂CO₃, NaOH, Bu₄NHSO₄ / benzene

5: 99 percent / TFA / CH₂Cl₂

6: 99 percent / pyridine

With pyridine; dmap; sodium hydroxide; aluminum amalgam; carbon dioxide; water; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; triphenylphosphine; trifluoroacetic acid; diethylazodicarboxylate; In tetrahydrofuran; diethyl ether; dichloromethane; acetonitrile; benzene;
DOI:10.1039/a703008h